chloromethyl 1-(o-nitrobenzyl)-2-pyrryl ketimine hydrochloride

Base Information

Chemical Name:chloromethyl 1-(o-nitrobenzyl)-2-pyrryl ketimine hydrochloride
CAS No.:81729-76-2
Molecular Formula:C₁₃H₁₂ClN₃O₂*ClH
Molecular Weight:314.171
Hs Code.:

Synonyms:chloromethyl 1-(o-nitrobenzyl)-2-pyrryl ketimine hydrochloride

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Chemical Property of chloromethyl 1-(o-nitrobenzyl)-2-pyrryl ketimine hydrochloride

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Technology Process of chloromethyl 1-(o-nitrobenzyl)-2-pyrryl ketimine hydrochloride

There total 7 articles about chloromethyl 1-(o-nitrobenzyl)-2-pyrryl ketimine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 81729-45-5
1-(2-nitrobenzyl)-1H-pyrrole

: 107-14-2
chloroacetonitrile

: 81729-76-2
chloromethyl 1-(o-nitrobenzyl)-2-pyrryl ketimine hydrochloride

Guidance literature:: With hydrogenchloride; In diethyl ether; 10 degC, 3h, then r.t., overnight;
DOI:10.1002/jhet.5570200626

Reference yield:

: 88-72-2
1-methyl-2-nitrobenzene

: 81729-76-2
chloromethyl 1-(o-nitrobenzyl)-2-pyrryl ketimine hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 1. Br₂ / Ambient temperature; 1. CCl₄, irradiation, reflux, 4h; 2. r.t., overnight

2: 12N hydrochloric acid / ethanol / Ambient temperature; overnight

3: 86 percent / acetic acid / 0.08 h / Heating

4: 64 percent / HCl (g) / diethyl ether / 10 degC, 3h, then r.t., overnight

With hydrogenchloride; bromine; In diethyl ether; ethanol; acetic acid;
DOI:10.1002/jhet.5570200626

Reference yield:

: 1904-78-5
2-nitrobenzylamine

: 81729-76-2
chloromethyl 1-(o-nitrobenzyl)-2-pyrryl ketimine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / acetic acid / 0.08 h / Heating

2: 64 percent / HCl (g) / diethyl ether / 10 degC, 3h, then r.t., overnight

With hydrogenchloride; In diethyl ether; acetic acid;
DOI:10.1002/jhet.5570200626