5-Acetylamino-1-benzyl-6-oxo-1,4,5,6-tetrahydro-pyridine-2,3-dicarboxylic acid dimethyl ester

Base Information

Chemical Name:5-Acetylamino-1-benzyl-6-oxo-1,4,5,6-tetrahydro-pyridine-2,3-dicarboxylic acid dimethyl ester
CAS No.:185856-21-7
Molecular Formula:C₁₈H₂₀N₂O₆
Molecular Weight:360.367
Hs Code.:

Synonyms:5-Acetylamino-1-benzyl-6-oxo-1,4,5,6-tetrahydro-pyridine-2,3-dicarboxylic acid dimethyl ester

Suppliers and Price of 5-Acetylamino-1-benzyl-6-oxo-1,4,5,6-tetrahydro-pyridine-2,3-dicarboxylic acid dimethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Acetylamino-1-benzyl-6-oxo-1,4,5,6-tetrahydro-pyridine-2,3-dicarboxylic acid dimethyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 5-Acetylamino-1-benzyl-6-oxo-1,4,5,6-tetrahydro-pyridine-2,3-dicarboxylic acid dimethyl ester

There total 3 articles about 5-Acetylamino-1-benzyl-6-oxo-1,4,5,6-tetrahydro-pyridine-2,3-dicarboxylic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 762-42-5
dimethyl acetylenedicarboxylate

: 185856-21-7
5-Acetylamino-1-benzyl-6-oxo-1,4,5,6-tetrahydro-pyridine-2,3-dicarboxylic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: BF₃*OEt₂ / tetrahydrofuran / Ambient temperature

2: EtO₂CCl / tetrahydrofuran / 14 h / Ambient temperature

With boron trifluoride diethyl etherate; chloroformic acid ethyl ester; In tetrahydrofuran;
DOI:10.1021/jo9600520

Reference yield:

: 100-46-9
benzylamine

: 185856-21-7
5-Acetylamino-1-benzyl-6-oxo-1,4,5,6-tetrahydro-pyridine-2,3-dicarboxylic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: BF₃*OEt₂ / tetrahydrofuran / Ambient temperature

2: EtO₂CCl / tetrahydrofuran / 14 h / Ambient temperature

With boron trifluoride diethyl etherate; chloroformic acid ethyl ester; In tetrahydrofuran;
DOI:10.1021/jo9600520

Reference yield:

: 4916-26-1
(Z)-<1,2-bis(methoxycarbonyl)vinyl>aminotoluene

: Sodium; 2-acetylamino-acrylate

: 185856-21-7
5-Acetylamino-1-benzyl-6-oxo-1,4,5,6-tetrahydro-pyridine-2,3-dicarboxylic acid dimethyl ester

Guidance literature:: With chloroformic acid ethyl ester; In tetrahydrofuran; for 14h; Yield given; Ambient temperature;
DOI:10.1021/jo9600520