(4R,5S,6S,7R)-4,7-Dibenzyl-1,3-bis-cyclopropylmethyl-5,6-bis-(2-trimethylsilanyl-ethoxymethoxy)-[1,3]diazepan-2-ylidene-cyanamide

Base Information

Chemical Name:(4R,5S,6S,7R)-4,7-Dibenzyl-1,3-bis-cyclopropylmethyl-5,6-bis-(2-trimethylsilanyl-ethoxymethoxy)-[1,3]diazepan-2-ylidene-cyanamide
CAS No.:153181-56-7
Molecular Formula:C₄₀H₆₂N₄O₄Si₂
Molecular Weight:719.128
Hs Code.:

Synonyms:(4R,5S,6S,7R)-4,7-Dibenzyl-1,3-bis-cyclopropylmethyl-5,6-bis-(2-trimethylsilanyl-ethoxymethoxy)-[1,3]diazepan-2-ylidene-cyanamide

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Chemical Property of (4R,5S,6S,7R)-4,7-Dibenzyl-1,3-bis-cyclopropylmethyl-5,6-bis-(2-trimethylsilanyl-ethoxymethoxy)-[1,3]diazepan-2-ylidene-cyanamide

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Technology Process of (4R,5S,6S,7R)-4,7-Dibenzyl-1,3-bis-cyclopropylmethyl-5,6-bis-(2-trimethylsilanyl-ethoxymethoxy)-[1,3]diazepan-2-ylidene-cyanamide

There total 5 articles about (4R,5S,6S,7R)-4,7-Dibenzyl-1,3-bis-cyclopropylmethyl-5,6-bis-(2-trimethylsilanyl-ethoxymethoxy)-[1,3]diazepan-2-ylidene-cyanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76513-69-4
(2-trimethylethylsilylethoxy)methyl chloride

: 153181-56-7
(4R,5S,6S,7R)-4,7-Dibenzyl-1,3-bis-cyclopropylmethyl-5,6-bis-(2-trimethylsilanyl-ethoxymethoxy)-[1,3]diazepan-2-ylidene-cyanamide

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / diisopropylethylamine / dimethylformamide / 16 h / Ambient temperature

2: 99 percent / H₂ / 5percent Pd/C / ethanol / 1.5 h

3: 60.9 percent / pyridine / 2 h / 125 °C

4: 1.) NaH / 1.) DMF, RT, 30 min, 2.) DMF, RT, 18 h

With pyridine; hydrogen; sodium hydride; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm970524i

Reference yield:

: 153223-10-0
(2R,3S,4S,5R)-2,5-bis[N-(benzyloxycarbonyl)amino]-1,6-diphenyl-3,4-hexanediol

: 153181-56-7
(4R,5S,6S,7R)-4,7-Dibenzyl-1,3-bis-cyclopropylmethyl-5,6-bis-(2-trimethylsilanyl-ethoxymethoxy)-[1,3]diazepan-2-ylidene-cyanamide

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / diisopropylethylamine / dimethylformamide / 16 h / Ambient temperature

2: 99 percent / H₂ / 5percent Pd/C / ethanol / 1.5 h

3: 60.9 percent / pyridine / 2 h / 125 °C

4: 1.) NaH / 1.) DMF, RT, 30 min, 2.) DMF, RT, 18 h

With pyridine; hydrogen; sodium hydride; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm970524i

Reference yield:

: 153181-18-1
dibenzyl ((2R,3S,4S,5R)-1,6-diphenyl-3,4-bis((2-(trimethylsilyl)ethoxy)methoxy)hexane-2,5-diyl)dicarbamate

: 153181-56-7
(4R,5S,6S,7R)-4,7-Dibenzyl-1,3-bis-cyclopropylmethyl-5,6-bis-(2-trimethylsilanyl-ethoxymethoxy)-[1,3]diazepan-2-ylidene-cyanamide

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / H₂ / 5percent Pd/C / ethanol / 1.5 h

2: 60.9 percent / pyridine / 2 h / 125 °C

3: 1.) NaH / 1.) DMF, RT, 30 min, 2.) DMF, RT, 18 h

With pyridine; hydrogen; sodium hydride; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm970524i