(6-(2-hydroxy-4-methoxyphenyl)-1H-tetrazol-1-yl)-2,3,4-trimethoxyphenol

Base Information

Chemical Name:(6-(2-hydroxy-4-methoxyphenyl)-1H-tetrazol-1-yl)-2,3,4-trimethoxyphenol
CAS No.:1448816-22-5
Molecular Formula:C₁₇H₁₈N₄O₆
Molecular Weight:374.353
Hs Code.:

Synonyms:(6-(2-hydroxy-4-methoxyphenyl)-1H-tetrazol-1-yl)-2,3,4-trimethoxyphenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (6-(2-hydroxy-4-methoxyphenyl)-1H-tetrazol-1-yl)-2,3,4-trimethoxyphenol

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Technology Process of (6-(2-hydroxy-4-methoxyphenyl)-1H-tetrazol-1-yl)-2,3,4-trimethoxyphenol

There total 13 articles about (6-(2-hydroxy-4-methoxyphenyl)-1H-tetrazol-1-yl)-2,3,4-trimethoxyphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1448816-36-1
1-(2-(benzyloxy)-3,4,5-trimethoxyphenyl)-5-(2-(benzyloxy)-4-methoxyphenyl)-1H-tetrazole

: 1448816-22-5
(6-(2-hydroxy-4-methoxyphenyl)-1H-tetrazol-1-yl)-2,3,4-trimethoxyphenol

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; for 7h; under 3102.97 Torr;
DOI:10.1016/j.bmcl.2013.06.004

Reference yield:

: (2-benzyloxy)-4-methoxybenzoylchloride

: 1448816-22-5
(6-(2-hydroxy-4-methoxyphenyl)-1H-tetrazol-1-yl)-2,3,4-trimethoxyphenol

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 12 h / 20 °C / Inert atmosphere

2: oxalyl dichloride; pyridine / dichloromethane / 4 h / 20 °C / Inert atmosphere

3: sodium azide / N,N-dimethyl-formamide / 4 h / 60 °C / Inert atmosphere

4: palladium 10% on activated carbon; hydrogen / methanol / 7 h / 3102.97 Torr

With pyridine; sodium azide; oxalyl dichloride; palladium 10% on activated carbon; hydrogen; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.06.004

Reference yield:

: C₃₁H₃₀ClNO₆

: 1448816-22-5
(6-(2-hydroxy-4-methoxyphenyl)-1H-tetrazol-1-yl)-2,3,4-trimethoxyphenol

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / N,N-dimethyl-formamide / 4 h / 60 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / methanol / 7 h / 3102.97 Torr

With sodium azide; palladium 10% on activated carbon; hydrogen; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.06.004