C₂₈H₃₆N₆O₄

Base Information

Chemical Name:C₂₈H₃₆N₆O₄
CAS No.:1346245-84-8
Molecular Formula:C₂₈H₃₆N₆O₄
Molecular Weight:520.632
Hs Code.:

C<sub>28</sub>H<sub>36</sub>N<sub>6</sub>O<sub>4</sub>

Synonyms:C₂₈H₃₆N₆O₄

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Chemical Property of C₂₈H₃₆N₆O₄

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Technology Process of C₂₈H₃₆N₆O₄

There total 9 articles about C₂₈H₃₆N₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 1346245-83-7
C₂₆H₃₁N₅O₇S

: 75-31-0
isopropylamine

: 1346245-84-8
C₂₈H₃₆N₆O₄

Guidance literature:: In acetonitrile; at 100 ℃; for 18h; sealed vessel;

Reference yield:

: 855400-66-7
3-bromo-5-methoxyphenol

: 1346245-84-8
C₂₈H₃₆N₆O₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 10 - 20 °C / Inert atmosphere

2.1: sodium t-butanolate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,2-dimethoxyethane / 2 h / 90 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 5 °C / Inert atmosphere

3.2: 15 h / 5 - 20 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 15 h / 20 °C

4.2: Cooling with ice

5.1: triethylamine / dichloromethane / 2 h / 5 - 10 °C / Inert atmosphere

6.1: acetonitrile / 18 h / 100 °C / sealed vessel

With tetrabutyl ammonium fluoride; sodium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium t-butanolate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; N,N-dimethyl-formamide; acetonitrile; mineral oil;

Reference yield:

: 1346245-42-8
C₁₁H₁₅BrO₄

: 1346245-84-8
C₂₈H₃₆N₆O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium t-butanolate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,2-dimethoxyethane / 2 h / 90 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 5 °C / Inert atmosphere

2.2: 15 h / 5 - 20 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 15 h / 20 °C

3.2: Cooling with ice

4.1: triethylamine / dichloromethane / 2 h / 5 - 10 °C / Inert atmosphere

5.1: acetonitrile / 18 h / 100 °C / sealed vessel

With tetrabutyl ammonium fluoride; sodium hydride; triethylamine; sodium t-butanolate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; N,N-dimethyl-formamide; acetonitrile; mineral oil;