4-amino-2-hydroxy-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)benzenesulfonamide hydrochloride

Base Information

Chemical Name:4-amino-2-hydroxy-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)benzenesulfonamide hydrochloride
CAS No.:1308254-68-3
Molecular Formula:C₁₃H₁₃BN₂O₅S*ClH
Molecular Weight:356.595
Hs Code.:

Synonyms:4-amino-2-hydroxy-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)benzenesulfonamide hydrochloride

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Chemical Property of 4-amino-2-hydroxy-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)benzenesulfonamide hydrochloride

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Technology Process of 4-amino-2-hydroxy-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)benzenesulfonamide hydrochloride

There total 4 articles about 4-amino-2-hydroxy-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)benzenesulfonamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1308255-82-4
2-hydroxy-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-4-nitrobenzenesulfonamide

: 1308254-68-3
4-amino-2-hydroxy-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)benzenesulfonamide hydrochloride

Guidance literature:: 2-hydroxy-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-4-nitrobenzenesulfonamide; With hydrogen; palladium 10% on activated carbon; In ethanol; at 20 ℃; for 3h; under 2585.81 Torr;

With hydrogenchloride;

Reference yield:

: 21320-91-2
2-methoxy-4-nitrobenzene-1-sulfonyl chloride

: 1308254-68-3
4-amino-2-hydroxy-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)benzenesulfonamide hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / acetonitrile / 20 °C

2: boron tribromide / dichloromethane / 20 °C

3: hydrogen / palladium 10% on activated carbon / ethanol / 3 h / 20 °C / 2585.81 Torr

With pyridine; hydrogen; boron tribromide; palladium 10% on activated carbon; In ethanol; dichloromethane; acetonitrile;

Reference yield:

: 117098-94-9
(5-amino-2-hydroxymethylphenyl)boronic acid

: 1308254-68-3
4-amino-2-hydroxy-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)benzenesulfonamide hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / acetonitrile / 20 °C

2: boron tribromide / dichloromethane / 20 °C

3: hydrogen / palladium 10% on activated carbon / ethanol / 3 h / 20 °C / 2585.81 Torr

With pyridine; hydrogen; boron tribromide; palladium 10% on activated carbon; In ethanol; dichloromethane; acetonitrile;