<(3S,5S,6S)-3-acetoxy-5,6-dihydroxy-5,6-dihydro-β-ionyliden>essigsaeure-aethylester

Base Information

Chemical Name:<(3S,5S,6S)-3-acetoxy-5,6-dihydroxy-5,6-dihydro-β-ionyliden>essigsaeure-aethylester
CAS No.:96193-05-4
Molecular Formula:C₁₉H₃₀O₆
Molecular Weight:354.444
Hs Code.:

Synonyms:<(3S,5S,6S)-3-acetoxy-5,6-dihydroxy-5,6-dihydro-β-ionyliden>essigsaeure-aethylester

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Chemical Property of <(3S,5S,6S)-3-acetoxy-5,6-dihydroxy-5,6-dihydro-β-ionyliden>essigsaeure-aethylester

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Technology Process of <(3S,5S,6S)-3-acetoxy-5,6-dihydroxy-5,6-dihydro-β-ionyliden>essigsaeure-aethylester

There total 3 articles about <(3S,5S,6S)-3-acetoxy-5,6-dihydroxy-5,6-dihydro-β-ionyliden>essigsaeure-aethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 96193-17-8
<(3S,5R,6S)-3-acetoxy-5,6-epoxy-5,6-dihydro-β-ionyliden>essigsaueure-aethylester

: 96193-05-4
<(3S,5S,6S)-3-acetoxy-5,6-dihydroxy-5,6-dihydro-β-ionyliden>essigsaeure-aethylester

: 96140-12-4
<(3S,5R,6R)-3-acetoxy-5,6-dihydroxy-5,6-dihydro-β-ionyliden>essigsaeure-aethylester

Guidance literature:: With sulfuric acid; In water; acetonitrile; for 1.45h; Ambient temperature;
DOI:10.1002/hlca.19840670804

Reference yield:

: 50281-41-9
(3S,5S,6S)-3-acetoxy-5,6-epoxy-5,6-dihydro-β-ionon

: 96193-05-4
<(3S,5S,6S)-3-acetoxy-5,6-dihydroxy-5,6-dihydro-β-ionyliden>essigsaeure-aethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / NaH / hexane; tetrahydrofuran / 20 h / Ambient temperature

2: 36 percent / H₂SO₄ / acetonitrile; H₂O / 1.45 h / Ambient temperature

With sulfuric acid; sodium hydride; In tetrahydrofuran; hexane; water; acetonitrile;
DOI:10.1002/hlca.19840670804

Reference yield:

: 54165-55-8
(3R)-3-Acetoxy-β-ionon

: 96193-05-4
<(3S,5S,6S)-3-acetoxy-5,6-dihydroxy-5,6-dihydro-β-ionyliden>essigsaeure-aethylester

Guidance literature:: Multi-step reaction with 3 steps

1: m-chloroperbenzoic acid / CHCl₃ / 0 deg C, 5 h; RT, 20 h

2: 71 percent / NaH / hexane; tetrahydrofuran / 20 h / Ambient temperature

3: 36 percent / H₂SO₄ / acetonitrile; H₂O / 1.45 h / Ambient temperature

With sulfuric acid; sodium hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; hexane; chloroform; water; acetonitrile;
DOI:10.1002/hlca.19840670804