{(meso-tetrakis-3,4,5-trimethoxyphenylporphyrin)bis(tert-butylamine)osmium(II)}

Base Information

Chemical Name:{(meso-tetrakis-3,4,5-trimethoxyphenylporphyrin)bis(tert-butylamine)osmium(II)}
CAS No.:139665-09-1
Molecular Formula:C₆₄H₇₄N₆O₁₂Os
Molecular Weight:1309.52
Hs Code.:

Synonyms:{(meso-tetrakis-3,4,5-trimethoxyphenylporphyrin)bis(tert-butylamine)osmium(II)}

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Chemical Property of {(meso-tetrakis-3,4,5-trimethoxyphenylporphyrin)bis(tert-butylamine)osmium(II)}

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Technology Process of {(meso-tetrakis-3,4,5-trimethoxyphenylporphyrin)bis(tert-butylamine)osmium(II)}

There total 2 articles about {(meso-tetrakis-3,4,5-trimethoxyphenylporphyrin)bis(tert-butylamine)osmium(II)} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: [(dinitrogen)Os(meso-tetrakis(3,4,5-trimethoxyphenyl)porphyrinato)(THF)]

: 75-64-9
tert-butylamine

: 139665-09-1
{(meso-tetrakis-3,4,5-trimethoxyphenylporphyrin)bis(tert-butylamine)osmium(II)}

Guidance literature:: In tetrahydrofuran; byproducts: N2; N2-atmosphere; excess amine, refluxing for 10 min; evapn., dissoln. in CHCl3, chromy. (Al2O3, CHCl3), concn., pptn. on pentane addn.; elem. anal.;

Reference yield:

: 140680-38-2
Os{(C₄H₂N)4(C(C₆H₂(OCH₃)3))4(N₂)(C₄H₈O)}

: 75-64-9
tert-butylamine

: 139665-09-1
{(meso-tetrakis-3,4,5-trimethoxyphenylporphyrin)bis(tert-butylamine)osmium(II)}

Guidance literature:: excess of tert-butylamine at room temp.; elem. anal.;
DOI:10.1039/c39920000161

Reference yield: 88.0%

: 139665-09-1
{(meso-tetrakis-3,4,5-trimethoxyphenylporphyrin)bis(tert-butylamine)osmium(II)}

: 139654-55-0
{(meso-tetrakis-3,4,5-trimethoxyphenylporphyrin)(dioxo)osmium(VI)}

: {(meso-tetrakis-3,4,5-trimethoxyphenylporphyrin)(tert-butylimido)(oxo)osmium(VI)}

Guidance literature:: With air; In tetrahydrofuran; stirring for 48 h; solvent removal, dissoln. in CH2Cl2, chromy. (Al2O3, CH2Cl2, then CHCl3/CH2Cl2=1:1), evapn., recrystn. (CH2Cl2/heptane); elem. anal.;