(Z)-benzyl 3-(3,4-dichlorophenyl)-3-methoxyallyl(2-(methoxymethyl)allyl)carbamate

Base Information

Chemical Name:(Z)-benzyl 3-(3,4-dichlorophenyl)-3-methoxyallyl(2-(methoxymethyl)allyl)carbamate
CAS No.:1398654-58-4
Molecular Formula:C₂₃H₂₅Cl₂NO₄
Molecular Weight:450.362
Hs Code.:

Synonyms:(Z)-benzyl 3-(3,4-dichlorophenyl)-3-methoxyallyl(2-(methoxymethyl)allyl)carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-benzyl 3-(3,4-dichlorophenyl)-3-methoxyallyl(2-(methoxymethyl)allyl)carbamate

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Technology Process of (Z)-benzyl 3-(3,4-dichlorophenyl)-3-methoxyallyl(2-(methoxymethyl)allyl)carbamate

There total 4 articles about (Z)-benzyl 3-(3,4-dichlorophenyl)-3-methoxyallyl(2-(methoxymethyl)allyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 1313875-02-3
benzyl 3-(3,4-dichlorophenyl)prop-2-ynyl(2-(methoxymethyl)allyl)carbamate

: 1398654-58-4
(Z)-benzyl 3-(3,4-dichlorophenyl)-3-methoxyallyl(2-(methoxymethyl)allyl)carbamate

Guidance literature:: With silver tetrafluoroborate; (triphenyl phosphite)gold(I) chloride; In methanol; dichloromethane; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ja303641p

Reference yield:

: 1315314-20-5
benzyl 2-(methoxymethyl)allyl(prop-2-ynyl)carbamate

: 1398654-58-4
(Z)-benzyl 3-(3,4-dichlorophenyl)-3-methoxyallyl(2-(methoxymethyl)allyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / N,N-dimethyl-formamide / 5 h / Inert atmosphere

2: silver tetrafluoroborate; (triphenyl phosphite)gold(I) chloride / methanol; dichloromethane / 24 h / 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; silver tetrafluoroborate; (triphenyl phosphite)gold(I) chloride; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide; 1: |Sonogashira Cross-Coupling;
DOI:10.1021/ja303641p

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 1398654-58-4
(Z)-benzyl 3-(3,4-dichlorophenyl)-3-methoxyallyl(2-(methoxymethyl)allyl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydrogencarbonate / 1 h / Inert atmosphere

1.2: 13 h / 0 - 20 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0 °C / Inert atmosphere

3.1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / N,N-dimethyl-formamide / 5 h / Inert atmosphere

4.1: silver tetrafluoroborate; (triphenyl phosphite)gold(I) chloride / methanol; dichloromethane / 24 h / 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; silver tetrafluoroborate; (triphenyl phosphite)gold(I) chloride; sodium hydride; sodium hydrogencarbonate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; 3.1: |Sonogashira Cross-Coupling;
DOI:10.1021/ja303641p