benzyl 3-(3,4-dichlorophenyl)prop-2-ynyl(2-(methoxymethyl)allyl)carbamate

Base Information

Chemical Name:benzyl 3-(3,4-dichlorophenyl)prop-2-ynyl(2-(methoxymethyl)allyl)carbamate
CAS No.:1313875-02-3
Molecular Formula:C₂₂H₂₁Cl₂NO₃
Molecular Weight:418.32
Hs Code.:

Synonyms:benzyl 3-(3,4-dichlorophenyl)prop-2-ynyl(2-(methoxymethyl)allyl)carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 3-(3,4-dichlorophenyl)prop-2-ynyl(2-(methoxymethyl)allyl)carbamate

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Technology Process of benzyl 3-(3,4-dichlorophenyl)prop-2-ynyl(2-(methoxymethyl)allyl)carbamate

There total 6 articles about benzyl 3-(3,4-dichlorophenyl)prop-2-ynyl(2-(methoxymethyl)allyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1315314-20-5
benzyl 2-(methoxymethyl)allyl(prop-2-ynyl)carbamate

: 20555-91-3
3,4-dichloroiodobenzene

: 1313875-02-3
benzyl 3-(3,4-dichlorophenyl)prop-2-ynyl(2-(methoxymethyl)allyl)carbamate

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1002/chem.201101346

Reference yield:

: C₁₄H₁₅Cl₂NO

: 501-53-1,94274-21-2
benzyl chloroformate

: 1313875-02-3
benzyl 3-(3,4-dichlorophenyl)prop-2-ynyl(2-(methoxymethyl)allyl)carbamate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1016/j.tetlet.2011.05.005

Reference yield:

: 886883-34-7
3-chloro-2-[(methyloxy)methyl]-1-propene

: 1313875-02-3
benzyl 3-(3,4-dichlorophenyl)prop-2-ynyl(2-(methoxymethyl)allyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 5 h / 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sodium hydride; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; 2: Sonogashira coupling;
DOI:10.1002/chem.201101346