bis(allyl)propionic acid

Base Information

Chemical Name:bis(allyl)propionic acid
CAS No.:1315320-40-1
Molecular Formula:C₉H₁₄O₂
Molecular Weight:154.209
Hs Code.:

Synonyms:bis(allyl)propionic acid

Suppliers and Price of bis(allyl)propionic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(allyl)propionic acid

Chemical Property:

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Technology Process of bis(allyl)propionic acid

There total 1 articles about bis(allyl)propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99-67-2
2-allyl-4-pentenoic acid

: 74-88-4
methyl iodide

: 1315320-40-1
bis(allyl)propionic acid

Guidance literature:: 2-allyl-4-pentenoic acid; With lithium diisopropyl amide; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

methyl iodide; at -78 - 20 ℃;
DOI:10.1021/ja204255e

Reference yield:

: 1315320-40-1
bis(allyl)propionic acid

: 1315320-19-4
C₁₅H₁₉NO₂

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 0.92 h / 0 - 20 °C / Inert atmosphere

2: diethyl ether; water / 0 °C

With oxalyl dichloride; In diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja204255e

Reference yield:

: 1315320-40-1
bis(allyl)propionic acid

: 1315320-20-7
C₂₃H₃₃N₃O₆

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 0.92 h / 0 - 20 °C / Inert atmosphere

2: diethyl ether; water / 0 °C

3: dimethyl sulfoxide / 19 h / 60 °C / 760.05 Torr / Inert atmosphere

With oxalyl dichloride; In diethyl ether; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/ja204255e