C₁₁H₁₂Br₂ClN

Base Information

• Chemical Name: C₁₁H₁₂Br₂ClN
• CAS No.: 1281963-93-6
• Molecular Formula: C₁₁H₁₂Br₂ClN
• Molecular Weight: 353.484
• Mol file: 1281963-93-6.mol

Synonyms:C₁₁H₁₂Br₂ClN

Chemical Property of C₁₁H₁₂Br₂ClN

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₁₁H₁₂Br₂ClN

There total 1 articles about C₁₁H₁₂Br₂ClN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

3,4-dibromo-3-methyl-1-butene (64251-92-9) + 2-CHLOROBENZYLAMINE (89-97-4) → C11H12Br2ClN (1281963-93-6)

Guidance literature:

With titanium tetrachloride; triethylamine; In diethyl ether; at 0 - 20 ℃; for 4h;

DOI:10.1021/jo102555r

Reference yield: 85.0%

C11H12Br2ClN (1281963-93-6) → 2-bromomethyl-1-(2-chlorobenzyl)-2-methylaziridine (1281964-01-9)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 0 - 20 ℃; for 36h;

DOI:10.1021/jo102555r

Reference yield:

C11H12Br2ClN (1281963-93-6) → 1-(2-chlorobenzyl)-3-methoxy-3-methylazetidine (1281964-03-1)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 36 h / 0 - 20 °C

2: sodium tetrahydroborate / 48 h / 0 °C / Reflux

With sodium tetrahydroborate; In methanol;

DOI:10.1021/jo102555r

upstream raw materials:

3,4-dibromo-3-methyl-1-butene

2-CHLOROBENZYLAMINE

Downstream raw materials:

2-bromomethyl-1-(2-chlorobenzyl)-2-methylaziridine

1-(2-chlorobenzyl)-3-methoxy-3-methylazetidine