(2aα,4α)-1,2,2a,3,4,5-hexahydro-1-benzoyl-5-methoxy-N,N-dipropylbenzindol-4-amine

Base Information

Chemical Name:(2aα,4α)-1,2,2a,3,4,5-hexahydro-1-benzoyl-5-methoxy-N,N-dipropylbenzindol-4-amine
CAS No.:114943-13-4
Molecular Formula:C₂₅H₃₂N₂O₂
Molecular Weight:392.541
Hs Code.:

(2aα,4α)-1,2,2a,3,4,5-hexahydro-1-benzoyl-5-methoxy-N,N-dipropylbenz<cd>indol-4-amine

Synonyms:(2aα,4α)-1,2,2a,3,4,5-hexahydro-1-benzoyl-5-methoxy-N,N-dipropylbenzindol-4-amine

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Chemical Property of (2aα,4α)-1,2,2a,3,4,5-hexahydro-1-benzoyl-5-methoxy-N,N-dipropylbenzindol-4-amine

Chemical Property:

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Technology Process of (2aα,4α)-1,2,2a,3,4,5-hexahydro-1-benzoyl-5-methoxy-N,N-dipropylbenzindol-4-amine

There total 13 articles about (2aα,4α)-1,2,2a,3,4,5-hexahydro-1-benzoyl-5-methoxy-N,N-dipropylbenzindol-4-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 107-08-4
1-iodo-propane

: 114943-11-2
(2aα,4α)-1,2,2a,3,4,5-hexahydro-1-benzoyl-5-methoxybenzindol-4-amine

: 114943-13-4
(2aα,4α)-1,2,2a,3,4,5-hexahydro-1-benzoyl-5-methoxy-N,N-dipropylbenzindol-4-amine

Guidance literature:: With potassium carbonate; In acetonitrile;
DOI:10.1021/jm00117a013

Reference yield: 63.0%

: 123-38-6
propionaldehyde

: 114943-11-2
(2aα,4α)-1,2,2a,3,4,5-hexahydro-1-benzoyl-5-methoxybenzindol-4-amine

: 114943-13-4
(2aα,4α)-1,2,2a,3,4,5-hexahydro-1-benzoyl-5-methoxy-N,N-dipropylbenzindol-4-amine

Guidance literature:: With sodium cyanoborohydride; acetic acid; In acetonitrile; for 3h;
DOI:10.1021/jm00117a013

Reference yield:

: 100561-47-5
1,2,2a,3,4,5-hexahydro-1-benzoyl-5-methoxybenzindol-5-ol

: 114943-13-4
(2aα,4α)-1,2,2a,3,4,5-hexahydro-1-benzoyl-5-methoxy-N,N-dipropylbenzindol-4-amine

Guidance literature:: Multi-step reaction with 6 steps

1: 96 percent / Amberlyst-15 resin / toluene / 3 h / 110 °C

2: 86 percent / 3-chloroperoxybenzoic acid / CHCl₃ / 5 h

3: 87 percent / ZnI₂ / benzene / 1 h / Heating

4: 99 percent / hydroxylamine hydrochloride / pyridine; ethanol / 0.25 h / Heating

5: 41 percent / hydrogen, ammonia / Raney Ni / ethanol / 10 h / 100 °C / 38786.1 Torr

6: 75 percent / K₂CO₃ / acetonitrile

With amberlyst-15 resin; hydroxylamine hydrochloride; ammonia; hydrogen; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; zinc(II) iodide; nickel; In pyridine; ethanol; chloroform; toluene; acetonitrile; benzene;
DOI:10.1021/jm00117a013