9-[4-(4,7,10,13-tetrathia-1-azacyclopentadecyl)phenyl]-N-methylacridinium perchlorate

Base Information

• Chemical Name: 9-[4-(4,7,10,13-tetrathia-1-azacyclopentadecyl)phenyl]-N-methylacridinium perchlorate
• CAS No.: 1274772-36-9
• Molecular Formula: C₃₀H₃₅N₂S₄*ClO₄
• Molecular Weight: 651.336
• Mol file: 1274772-36-9.mol

Synonyms:9-[4-(4,7,10,13-tetrathia-1-azacyclopentadecyl)phenyl]-N-methylacridinium perchlorate

Chemical Property of 9-[4-(4,7,10,13-tetrathia-1-azacyclopentadecyl)phenyl]-N-methylacridinium perchlorate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 9-[4-(4,7,10,13-tetrathia-1-azacyclopentadecyl)phenyl]-N-methylacridinium perchlorate

There total 4 articles about 9-[4-(4,7,10,13-tetrathia-1-azacyclopentadecyl)phenyl]-N-methylacridinium perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-methylacridinium iodide (948-43-6) + 13-phenyl-1,4,7,10-tetrathia-13-azacyclopentadecane (148932-07-4) → 9-[4-(4,7,10,13-tetrathia-1-azacyclopentadecyl)phenyl]-N-methylacridinium perchlorate (1274772-36-9)

Guidance literature:

With iodine; In N,N-dimethyl-formamide;

DOI:10.1039/c0cp01411g

Reference yield:

2,2'-(phenylimino)bis[ethanol] (120-07-0) → 9-[4-(4,7,10,13-tetrathia-1-azacyclopentadecyl)phenyl]-N-methylacridinium perchlorate (1274772-36-9)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydroxide / tetrahydrofuran; water

2: caesium carbonate / N,N-dimethyl-formamide

3: iodine / N,N-dimethyl-formamide

With iodine; caesium carbonate; sodium hydroxide; In tetrahydrofuran; water; N,N-dimethyl-formamide;

DOI:10.1039/c0cp01411g

Reference yield:

N,N-bis(2-p-tolylsulfonyloxyethyl)aniline (3590-12-3) → 9-[4-(4,7,10,13-tetrathia-1-azacyclopentadecyl)phenyl]-N-methylacridinium perchlorate (1274772-36-9)

Guidance literature:

Multi-step reaction with 2 steps

1: caesium carbonate / N,N-dimethyl-formamide

2: iodine / N,N-dimethyl-formamide

With iodine; caesium carbonate; In N,N-dimethyl-formamide;

DOI:10.1039/c0cp01411g

upstream raw materials:

2,2'-(phenylimino)bis[ethanol]

N,N-bis(2-p-tolylsulfonyloxyethyl)aniline

N-methylacridinium iodide

13-phenyl-1,4,7,10-tetrathia-13-azacyclopentadecane