N-benzenesulphonyl-N-(3-{(R)-2-[3-(5-formyl-indol-1-yl)-1,1-dimethyl-propylamino]-1-hydroxy-ethyl}-phenyl)-benzenesulphonamide

Base Information

Chemical Name:N-benzenesulphonyl-N-(3-{(R)-2-[3-(5-formyl-indol-1-yl)-1,1-dimethyl-propylamino]-1-hydroxy-ethyl}-phenyl)-benzenesulphonamide
CAS No.:936004-18-1
Molecular Formula:C₃₄H₃₅N₃O₆S₂
Molecular Weight:645.8
Hs Code.:

Synonyms:N-benzenesulphonyl-N-(3-{(R)-2-[3-(5-formyl-indol-1-yl)-1,1-dimethyl-propylamino]-1-hydroxy-ethyl}-phenyl)-benzenesulphonamide

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Chemical Property of N-benzenesulphonyl-N-(3-{(R)-2-[3-(5-formyl-indol-1-yl)-1,1-dimethyl-propylamino]-1-hydroxy-ethyl}-phenyl)-benzenesulphonamide

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Technology Process of N-benzenesulphonyl-N-(3-{(R)-2-[3-(5-formyl-indol-1-yl)-1,1-dimethyl-propylamino]-1-hydroxy-ethyl}-phenyl)-benzenesulphonamide

There total 1 articles about N-benzenesulphonyl-N-(3-{(R)-2-[3-(5-formyl-indol-1-yl)-1,1-dimethyl-propylamino]-1-hydroxy-ethyl}-phenyl)-benzenesulphonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 936004-20-5
1-(3-amino-3-methylbutyl)-1H-indole-5-carbaldehyde

: 935854-34-5
N-[(R)-3-oxiranyl-phenyl]-dibenzenesulphonamide

: 936004-18-1
N-benzenesulphonyl-N-(3-{(R)-2-[3-(5-formyl-indol-1-yl)-1,1-dimethyl-propylamino]-1-hydroxy-ethyl}-phenyl)-benzenesulphonamide

Guidance literature:: In ethylene glycol; at 120 ℃; for 2.5h;

Reference yield: 73.0%

: 936004-18-1
N-benzenesulphonyl-N-(3-{(R)-2-[3-(5-formyl-indol-1-yl)-1,1-dimethyl-propylamino]-1-hydroxy-ethyl}-phenyl)-benzenesulphonamide

: 76-05-1
trifluoroacetic acid

: 936003-91-7
N-(3-{(R)-1-hydroxy-2-[3-(5-hydroxymethylindol-1-yl)-1,1-dimethylpropylamino]ethyl}phenyl)benzenesulphonamide hydrotrifluoroacetate

Guidance literature:: N-benzenesulphonyl-N-(3-{(R)-2-[3-(5-formyl-indol-1-yl)-1,1-dimethyl-propylamino]-1-hydroxy-ethyl}-phenyl)-benzenesulphonamide; With sodium tetrahydroborate; In methanol; at 20 ℃; for 1.16667h;

With sodium hydroxide; water; In methanol; N,N-dimethyl-formamide; at 20 ℃; for 2h;

trifluoroacetic acid;

Reference yield: 29.0%

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 936004-18-1
N-benzenesulphonyl-N-(3-{(R)-2-[3-(5-formyl-indol-1-yl)-1,1-dimethyl-propylamino]-1-hydroxy-ethyl}-phenyl)-benzenesulphonamide

: 76-05-1
trifluoroacetic acid

: (E)-3-(1-{3-[(R)-2-[3-(phenylsulphonylamino)-phenyl]-2-hydroxy-ethylamino]-3-methylbutyl}-1H-indol-5-yl)acrylic acid hydrotrifluoroacetate

Guidance literature:: diethoxyphosphoryl-acetic acid ethyl ester; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.0833333h;

N-benzenesulphonyl-N-(3-{(R)-2-[3-(5-formyl-indol-1-yl)-1,1-dimethyl-propylamino]-1-hydroxy-ethyl}-phenyl)-benzenesulphonamide; In tetrahydrofuran; at 0 - 20 ℃; for 69.0833h;

trifluoroacetic acid; With sodium hydroxide; ethanol; water; more than 3 stages;