1-(4-chloro-phenyl)-3-[4-(2-fluoro-phenyl)-5-mercapto-4H-[1,2,4]triazol-3-yl]-6-methyl-1H-pyridazin-4-one

Base Information

Chemical Name:1-(4-chloro-phenyl)-3-[4-(2-fluoro-phenyl)-5-mercapto-4H-[1,2,4]triazol-3-yl]-6-methyl-1H-pyridazin-4-one
CAS No.:374589-06-7
Molecular Formula:C₁₉H₁₃ClFN₅OS
Molecular Weight:413.863
Hs Code.:

1-(4-chloro-phenyl)-3-[4-(2-fluoro-phenyl)-5-mercapto-4<i>H</i>-[1,2,4]triazol-3-yl]-6-methyl-1<i>H</i>-pyridazin-4-one

Synonyms:1-(4-chloro-phenyl)-3-[4-(2-fluoro-phenyl)-5-mercapto-4H-[1,2,4]triazol-3-yl]-6-methyl-1H-pyridazin-4-one

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Chemical Property of 1-(4-chloro-phenyl)-3-[4-(2-fluoro-phenyl)-5-mercapto-4H-[1,2,4]triazol-3-yl]-6-methyl-1H-pyridazin-4-one

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Technology Process of 1-(4-chloro-phenyl)-3-[4-(2-fluoro-phenyl)-5-mercapto-4H-[1,2,4]triazol-3-yl]-6-methyl-1H-pyridazin-4-one

There total 3 articles about 1-(4-chloro-phenyl)-3-[4-(2-fluoro-phenyl)-5-mercapto-4H-[1,2,4]triazol-3-yl]-6-methyl-1H-pyridazin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.7%

: 355378-65-3
C₁₉H₁₅ClFN₅O₂S

: 374589-06-7
1-(4-chloro-phenyl)-3-[4-(2-fluoro-phenyl)-5-mercapto-4H-[1,2,4]triazol-3-yl]-6-methyl-1H-pyridazin-4-one

Guidance literature:: With sodium carbonate; for 5h; Heating;
DOI:10.1002/jhet.5570380431

Reference yield:

: 38985-64-7
o-fluorophenyl isothiocyanate

: 374589-06-7
1-(4-chloro-phenyl)-3-[4-(2-fluoro-phenyl)-5-mercapto-4H-[1,2,4]triazol-3-yl]-6-methyl-1H-pyridazin-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / ethanol / 3 h / Heating

2: 89.7 percent / aq. Na₂CO₃ / 5 h / Heating

With sodium carbonate; In ethanol;
DOI:10.1002/jhet.5570380431

Reference yield:

: 1-(4-chloro-phenyl)-6-methyl-4-oxo-1,4-dihydro-pyridazine-3-carboxylic acid hydrazide

: 374589-06-7
1-(4-chloro-phenyl)-3-[4-(2-fluoro-phenyl)-5-mercapto-4H-[1,2,4]triazol-3-yl]-6-methyl-1H-pyridazin-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / ethanol / 3 h / Heating

2: 89.7 percent / aq. Na₂CO₃ / 5 h / Heating

With sodium carbonate; In ethanol;
DOI:10.1002/jhet.5570380431