C₁₈H₂₄BrNO

Base Information

Chemical Name:C₁₈H₂₄BrNO
CAS No.:1398756-68-7
Molecular Formula:C₁₈H₂₄BrNO
Molecular Weight:350.299
Hs Code.:

Synonyms:C₁₈H₂₄BrNO

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Chemical Property of C₁₈H₂₄BrNO

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Technology Process of C₁₈H₂₄BrNO

There total 4 articles about C₁₈H₂₄BrNO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1398756-54-1
3-bromo-N,N-diallyl-4-hydroxymethyl aniline

: 870-63-3
prenyl bromide

: 1398756-68-7
C₁₈H₂₄BrNO

Guidance literature:: 3-bromo-N,N-diallyl-4-hydroxymethyl aniline; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; for 0.5h;

prenyl bromide; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; for 18h;
DOI:10.1021/ja306881u

Reference yield:

: 124-02-7
diallylamine

: 1398756-68-7
C₁₈H₂₄BrNO

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 19 h / 100 °C

2.1: methanol; lithium borohydride / tetrahydrofuran / 0 - 20 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 - 20 °C

3.2: 18 h / 0 - 20 °C

With methanol; lithium borohydride; sodium hydride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ja306881u

Reference yield:

: 653-92-9
methyl 2-bromo-4-fluorobenzoate

: 1398756-68-7
C₁₈H₂₄BrNO

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 19 h / 100 °C

2.1: methanol; lithium borohydride / tetrahydrofuran / 0 - 20 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 - 20 °C

3.2: 18 h / 0 - 20 °C

With methanol; lithium borohydride; sodium hydride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ja306881u