C₁₅H₂₈N₂O

Base Information

• Chemical Name: C₁₅H₂₈N₂O
• CAS No.: 1312953-70-0
• Molecular Formula: C₁₅H₂₈N₂O
• Molecular Weight: 252.4
• Mol file: 1312953-70-0.mol

Synonyms:C₁₅H₂₈N₂O

Chemical Property of C₁₅H₂₈N₂O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₂₈N₂O

There total 5 articles about C₁₅H₂₈N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C23H36N2O (1312953-69-7) → C15H28N2O (1312953-70-0)

Guidance literature:

With 20 % Pd(OH)2/C; hydrogen; In methanol; at 70 ℃; for 16h; under 4137.29 Torr;

DOI:10.1016/j.tet.2011.02.027

Reference yield:

C23H34N2 (1312953-68-6) → C15H28N2O (1312953-70-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sulfuric acid / 18 h / Inert atmosphere; Heating

1.2: 0 °C / Inert atmosphere

2.1: 20 % Pd(OH)2/C; hydrogen / methanol / 16 h / 70 °C / 4137.29 Torr

With sulfuric acid; 20 % Pd(OH)2/C; hydrogen; In methanol;

DOI:10.1016/j.tet.2011.02.027

Reference yield:

1,1-dicyclohexyl-2-hydroxy ethane (204844-09-7) → C15H28N2O (1312953-70-0)

Guidance literature:

Multi-step reaction with 4 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: hydrogenchloride / methanol; water / 124 h / 20 °C / Inert atmosphere

3.1: sulfuric acid / 18 h / Inert atmosphere; Heating

3.2: 0 °C / Inert atmosphere

4.1: 20 % Pd(OH)2/C; hydrogen / methanol / 16 h / 70 °C / 4137.29 Torr

With hydrogenchloride; oxalyl dichloride; sulfuric acid; 20 % Pd(OH)2/C; hydrogen; dimethyl sulfoxide; In methanol; dichloromethane; water;

DOI:10.1016/j.tet.2011.02.027

upstream raw materials:

1,1-dicyclohexyl-2-hydroxy ethane

C₂₃H₃₄N₂

C₂₃H₃₆N₂O

2,2-dicyclohexylacetaldehyde

Downstream raw materials:

C₁₅H₂₉NO

C₃₅H₆₂N₂O₄

C₃₅H₆₀Cl₂N₂O₂

C₃₅H₅₈N₂O₂