1,1-dicyclohexyl-2-hydroxy ethane

Base Information

• Chemical Name: 1,1-dicyclohexyl-2-hydroxy ethane
• CAS No.: 204844-09-7
• Molecular Formula: C₁₄H₂₆O
• Molecular Weight: 210.36
• Mol file: 204844-09-7.mol

Synonyms:1,1-dicyclohexyl-2-hydroxy ethane

Chemical Property of 1,1-dicyclohexyl-2-hydroxy ethane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,1-dicyclohexyl-2-hydroxy ethane

There total 2 articles about 1,1-dicyclohexyl-2-hydroxy ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dicyclohexylacetic acid (52034-92-1) → 1,1-dicyclohexyl-2-hydroxy ethane (204844-09-7)

Guidance literature:

dicyclohexylacetic acid; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 20h; Inert atmosphere; Reflux;

With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃; Inert atmosphere;

DOI:10.1016/j.tet.2011.02.027

Reference yield:

dicyclohexylacetic acid (52034-92-1) + water (7732-18-5) + sodium carbonate (497-19-8) → 1,1-dicyclohexyl-2-hydroxy ethane (204844-09-7)

Guidance literature:

With borane; In tetrahydrofuran;

Reference yield:

1,1-dicyclohexyl-2-hydroxy ethane (204844-09-7) → 2,2-dicyclohexylacetaldehyde (269071-95-6)

Guidance literature:

1,1-dicyclohexyl-2-hydroxy ethane; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; Inert atmosphere;

With triethylamine; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;

DOI:10.1016/j.tet.2011.02.027

upstream raw materials:

dicyclohexylacetic acid

water

sodium carbonate

Downstream raw materials:

C₂₃H₃₄N₂

C₂₃H₃₆N₂O

C₁₅H₂₈N₂O

C₁₅H₂₉NO