(C₅H₅)Re(NO)(P(C₆H₅)3)(CH₂O)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)Re(NO)(P(C₆H₅)3)(CH₂O)PF₆

Base Information

Chemical Name:(C₅H₅)Re(NO)(P(C₆H₅)3)(CH₂O)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)Re(NO)(P(C₆H₅)3)(CH₂O)PF₆
CAS No.:84369-16-4
Molecular Formula:C₂₄H₂₂NO₂PRe*F₆P
Molecular Weight:718.589
Hs Code.:

(C<sub>5</sub>H<sub>5</sub>)Re(NO)(P(C<sub>6</sub>H<sub>5</sub>)3)(CH<sub>2</sub>O)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=(C<sub>5</sub>H<sub>5</sub>)Re(NO)(P(C<sub>6</sub>H<sub>5</sub>)3)(CH<sub>2</sub>O)PF<sub>6</sub>

Synonyms:(C₅H₅)Re(NO)(P(C₆H₅)3)(CH₂O)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)Re(NO)(P(C₆H₅)3)(CH₂O)PF₆

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Chemical Property of (C₅H₅)Re(NO)(P(C₆H₅)3)(CH₂O)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)Re(NO)(P(C₆H₅)3)(CH₂O)PF₆

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Technology Process of (C₅H₅)Re(NO)(P(C₆H₅)3)(CH₂O)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)Re(NO)(P(C₆H₅)3)(CH₂O)PF₆

There total 3 articles about (C₅H₅)Re(NO)(P(C₆H₅)3)(CH₂O)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)Re(NO)(P(C₆H₅)3)(CH₂O)PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: (η5-C5H5)(Me)(NO)(PPh3)rhenium(II)

: 536-80-1
iodosylbenzene

: 437-17-2
tritylium hexafluorophosphate

: 84369-16-4
(C₅H₅)Re(NO)(P(C₆H₅)3)(CH₂O)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)Re(NO)(P(C₆H₅)3)(CH₂O)PF₆

Guidance literature:: In dichloromethane; byproducts: C6H5I; Ph3CPF6 was added to a soln. of Re complex at -78°C with stirring under N2, after 15 min iodosobenzene was added, the resulting suspn. was kept at -23°C for 3 h; filtn., concn., addn. of hexane, drying of ppt., purifn. by recrystn. from CH2Cl2-hexane; elem. anal.;