N-(cyclohex-2-enyl)-N-((2,3-diphenylcycloallyl)methyl)-4-methylbenzenesulfonamide

Base Information

• Chemical Name: N-(cyclohex-2-enyl)-N-((2,3-diphenylcycloallyl)methyl)-4-methylbenzenesulfonamide
• CAS No.: 1234210-34-4
• Molecular Formula: C₂₉H₂₉NO₂S
• Molecular Weight: 455.621
• Mol file: 1234210-34-4.mol

Synonyms:N-(cyclohex-2-enyl)-N-((2,3-diphenylcycloallyl)methyl)-4-methylbenzenesulfonamide

Chemical Property of N-(cyclohex-2-enyl)-N-((2,3-diphenylcycloallyl)methyl)-4-methylbenzenesulfonamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of N-(cyclohex-2-enyl)-N-((2,3-diphenylcycloallyl)methyl)-4-methylbenzenesulfonamide

There total 1 articles about N-(cyclohex-2-enyl)-N-((2,3-diphenylcycloallyl)methyl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

1,2-diphenyl-3-hydroxymethyl-1-cyclopropene (6415-73-2) + N-cyclohex-2-enyl-4-methyl-benzenesulfonamide (57981-18-7) → N-(cyclohex-2-enyl)-N-((2,3-diphenylcycloallyl)methyl)-4-methylbenzenesulfonamide (1234210-34-4)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere;

DOI:10.1021/ol101091r

Reference yield: 68.0%

carbon monoxide (201230-82-2) + N-(cyclohex-2-enyl)-N-((2,3-diphenylcycloallyl)methyl)-4-methylbenzenesulfonamide (1234210-34-4) → 3,4-diphenyl-1-tosyl-2,2a,2a1,5a,6,7,8,8a-octahydrobenzo[cd]indol-5(1H)-one

Guidance literature:

With di(rhodium)tetracarbonyl dichloride; In 1,2-dichloro-ethane; at 80 ℃; for 12h; under 760.051 Torr;

DOI:10.1021/ol101091r

upstream raw materials:

1,2-diphenyl-3-hydroxymethyl-1-cyclopropene

N-cyclohex-2-enyl-4-methyl-benzenesulfonamide