C₁₇H₂₃BrO

Base Information

Chemical Name:C₁₇H₂₃BrO
CAS No.:1393475-04-1
Molecular Formula:C₁₇H₂₃BrO
Molecular Weight:323.273
Hs Code.:

Synonyms:C₁₇H₂₃BrO

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Chemical Property of C₁₇H₂₃BrO

Chemical Property:

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Technology Process of C₁₇H₂₃BrO

There total 2 articles about C₁₇H₂₃BrO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 86636-47-7
(2Z,6Z)-8-(benzyloxy)-2,6-dimethyl-1-(tetrahydropyran-2-yloxy)-octa-2,6-diene

: 1393475-04-1
C₁₇H₂₃BrO

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid / methanol / 6 h / 20 °C / Inert atmosphere

2.1: methanesulfonic acid; triethylamine / tetrahydrofuran / 1 h / Cooling with ice; Inert atmosphere

2.2: 2 h / Cooling with ice; Inert atmosphere

With methanesulfonic acid; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; methanol;
DOI:10.1021/ja306184m

Reference yield:

: 52188-74-6,70238-38-9,94854-66-7,115425-27-9,130487-40-0,86636-48-8
(2Z,6Z)-8-(benzyloxy)-2,6-dimethylocta-2,6-dien-1-ol

: 1393475-04-1
C₁₇H₂₃BrO

Guidance literature:: (2Z,6Z)-8-(benzyloxy)-2,6-dimethylocta-2,6-dien-1-ol; With methanesulfonic acid; triethylamine; In tetrahydrofuran; for 1h; Cooling with ice; Inert atmosphere;

With lithium bromide; In tetrahydrofuran; for 2h; Cooling with ice; Inert atmosphere;
DOI:10.1021/ja306184m

Reference yield: 71.0%

: 1393475-04-1
C₁₇H₂₃BrO

: 68690-45-9,80370-68-9,53254-63-0
(2E,6E)-3,7,11-trimethyl-1-(p-tolylsulfonyl)dodeca-2,6,10-triene

: 68690-52-8,68738-08-9,92542-05-7
9-(R/S)-p-toluenesulfonyl-3,7,11,15,19-pentamethyleicosa-2Z,6Z,10E,14E,18-pentaen-1-ol benzyl ether

Guidance literature:: (2E,6E)-3,7,11-trimethyl-1-(p-tolylsulfonyl)dodeca-2,6,10-triene; With n-butyllithium; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; at -78 ℃; for 1.5h; Inert atmosphere;

C₁₇H₂₃BrO; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; at -78 ℃; for 6h; Inert atmosphere;
DOI:10.1021/ja306184m