2,5-bis(5-hexenyloxy)p-xylylene alcohol

Base Information

Chemical Name:2,5-bis(5-hexenyloxy)p-xylylene alcohol
CAS No.:865288-75-1
Molecular Formula:C₂₀H₃₀O₄
Molecular Weight:334.456
Hs Code.:

Synonyms:2,5-bis(5-hexenyloxy)p-xylylene alcohol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,5-bis(5-hexenyloxy)p-xylylene alcohol

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Technology Process of 2,5-bis(5-hexenyloxy)p-xylylene alcohol

There total 3 articles about 2,5-bis(5-hexenyloxy)p-xylylene alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 865288-74-0
diethyl 2,5-bis(5-hexenyloxy)terephthalate

: 865288-75-1
2,5-bis(5-hexenyloxy)p-xylylene alcohol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 1h; Heating;
DOI:10.1021/ma0508956

Reference yield:

: 5870-38-2
diethyl 2,5-(dihydroxy)terephthalate

: 865288-75-1
2,5-bis(5-hexenyloxy)p-xylylene alcohol

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / K₂CO₃ / dimethylformamide / 20 h / 80 °C

2: 82 percent / LiAlH₄ / diethyl ether / 1 h / Heating

With lithium aluminium tetrahydride; potassium carbonate; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/ma0508956

Reference yield:

: 2695-47-8
6-Bromo-1-hexene

: 865288-75-1
2,5-bis(5-hexenyloxy)p-xylylene alcohol

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / K₂CO₃ / dimethylformamide / 20 h / 80 °C

2: 82 percent / LiAlH₄ / diethyl ether / 1 h / Heating

With lithium aluminium tetrahydride; potassium carbonate; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/ma0508956