α-1-C-propargyl-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-tert-butoxycarboxylimino-D-xylitol

Base Information

• Chemical Name: α-1-C-propargyl-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-tert-butoxycarboxylimino-D-xylitol
• CAS No.: 1624966-37-5
• Molecular Formula: C₃₄H₃₉NO₅
• Molecular Weight: 541.687

Synonyms:α-1-C-propargyl-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-tert-butoxycarboxylimino-D-xylitol

Chemical Property of α-1-C-propargyl-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-tert-butoxycarboxylimino-D-xylitol

Chemical Property:

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Technology Process of α-1-C-propargyl-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-tert-butoxycarboxylimino-D-xylitol

There total 1 articles about α-1-C-propargyl-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-tert-butoxycarboxylimino-D-xylitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C33H39NO6 (1624966-58-0) + dimethyl 1-(1-diazo-2-oxopropyl)phosphonate (90965-06-3) → α-1-C-propargyl-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-tert-butoxycarboxylimino-D-xylitol (1624966-37-5)

Guidance literature:

With potassium carbonate; In methanol; at 20 ℃; for 5h;

DOI:10.1002/cmdc.201402023

Reference yield: 93.0%

α-1-C-propargyl-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-tert-butoxycarboxylimino-D-xylitol (1624966-37-5) → α-1-C-propargyl-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol (1624966-39-7)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1002/cmdc.201402023

Reference yield: 67.0%

α-1-C-propargyl-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-tert-butoxycarboxylimino-D-xylitol (1624966-37-5) → α-1-C-propargyl-1,5-dideoxy-1,5-imino-D-xylitol (1624966-36-4) + α-1-C-propargyl-2-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol (1624966-38-6)

Guidance literature:

With pentamethylbenzene,; boron trichloride; In dichloromethane; at -78 ℃; for 4h;

DOI:10.1002/cmdc.201402023

upstream raw materials:

C₃₃H₃₉NO₆

dimethyl 1-(1-diazo-2-oxopropyl)phosphonate

Downstream raw materials:

α-1-C-((1-benzyl-1H-1,2,3-triazol-4-yl)-methyl)-1,5-dideoxy-1,5-imino-D-xylitol

α-1-C-((1-benzyl-1H-1,2,3-triazol-4-yl)-methyl)-2-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol

α-1-C-propargyl-1,5-dideoxy-1,5-imino-D-xylitol

α-1-C-propargyl-2-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol

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