α-1-C-((1-benzyl-1H-1,2,3-triazol-4-yl)-methyl)-2-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol

Base Information

Chemical Name:α-1-C-((1-benzyl-1H-1,2,3-triazol-4-yl)-methyl)-2-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol
CAS No.:1624966-56-8
Molecular Formula:C₂₂H₂₆N₄O₃
Molecular Weight:394.473
Hs Code.:

Synonyms:α-1-C-((1-benzyl-1H-1,2,3-triazol-4-yl)-methyl)-2-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol

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Chemical Property of α-1-C-((1-benzyl-1H-1,2,3-triazol-4-yl)-methyl)-2-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol

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Technology Process of α-1-C-((1-benzyl-1H-1,2,3-triazol-4-yl)-methyl)-2-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol

There total 2 articles about α-1-C-((1-benzyl-1H-1,2,3-triazol-4-yl)-methyl)-2-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1624966-41-1
α-1-C-(1-benzyl-1H-1,2,3-triazol-4-yl)-methyl-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol

: 1624966-55-7
α-1-C-((1-benzyl-1H-1,2,3-triazol-4-yl)-methyl)-1,5-dideoxy-1,5-imino-D-xylitol

: 1624966-56-8
α-1-C-((1-benzyl-1H-1,2,3-triazol-4-yl)-methyl)-2-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol

Guidance literature:: With boron trichloride; In dichloromethane; at -60 - 0 ℃; for 3h;
DOI:10.1002/cmdc.201402023

Reference yield:

: 1624966-37-5
α-1-C-propargyl-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-tert-butoxycarboxylimino-D-xylitol

: 1624966-55-7
α-1-C-((1-benzyl-1H-1,2,3-triazol-4-yl)-methyl)-1,5-dideoxy-1,5-imino-D-xylitol

: 1624966-56-8
α-1-C-((1-benzyl-1H-1,2,3-triazol-4-yl)-methyl)-2-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

2: copper(ll) sulfate pentahydrate; Erythorbic acid / tetrahydrofuran; water / 15 h / 20 °C

3: boron trichloride / dichloromethane / 3 h / -60 - 0 °C

With copper(ll) sulfate pentahydrate; boron trichloride; Erythorbic acid; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water;
DOI:10.1002/cmdc.201402023