phenylthio 2-O-dimethyl-(1-O-methyl-2,4,6-tri-O-benzyl-α-D-glucopyranos-3-oxyl)-silyl-3,4,6-tri-O-acetyl-α-D-glucopyranoside

Base Information

Chemical Name:phenylthio 2-O-dimethyl-(1-O-methyl-2,4,6-tri-O-benzyl-α-D-glucopyranos-3-oxyl)-silyl-3,4,6-tri-O-acetyl-α-D-glucopyranoside
CAS No.:150592-42-0
Molecular Formula:C₄₈H₅₈O₁₄SSi
Molecular Weight:919.132
Hs Code.:

Synonyms:phenylthio 2-O-dimethyl-(1-O-methyl-2,4,6-tri-O-benzyl-α-D-glucopyranos-3-oxyl)-silyl-3,4,6-tri-O-acetyl-α-D-glucopyranoside

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Chemical Property of phenylthio 2-O-dimethyl-(1-O-methyl-2,4,6-tri-O-benzyl-α-D-glucopyranos-3-oxyl)-silyl-3,4,6-tri-O-acetyl-α-D-glucopyranoside

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Technology Process of phenylthio 2-O-dimethyl-(1-O-methyl-2,4,6-tri-O-benzyl-α-D-glucopyranos-3-oxyl)-silyl-3,4,6-tri-O-acetyl-α-D-glucopyranoside

There total 2 articles about phenylthio 2-O-dimethyl-(1-O-methyl-2,4,6-tri-O-benzyl-α-D-glucopyranos-3-oxyl)-silyl-3,4,6-tri-O-acetyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 143206-82-0
phenyl 3,4,6-tri-O-acetyl-α-D-gluco-1-thiopyranoside

: 150592-41-9
methyl 3-O-chlorodimethylsilyl-2,4,6-tri-O-benzyl-α-D-glucopyranoside

: 150592-42-0
phenylthio 2-O-dimethyl-(1-O-methyl-2,4,6-tri-O-benzyl-α-D-glucopyranos-3-oxyl)-silyl-3,4,6-tri-O-acetyl-α-D-glucopyranoside

Guidance literature:: With pyridine; In tetrahydrofuran;
DOI:10.1039/c39930000791

Reference yield:

: 35303-86-7
(2R,3S,4S,5R,6S)-3,5-Bis-benzyloxy-2-benzyloxymethyl-6-methoxy-tetrahydro-pyran-4-ol

: 150592-42-0
phenylthio 2-O-dimethyl-(1-O-methyl-2,4,6-tri-O-benzyl-α-D-glucopyranos-3-oxyl)-silyl-3,4,6-tri-O-acetyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / Et₃N / diethyl ether / 0.17 h / 0 °C

2: 66 percent / pyridine / tetrahydrofuran / 2 h / 25 °C

With pyridine; triethylamine; In tetrahydrofuran; diethyl ether;
DOI:10.1016/S0040-4020(01)80200-3