bis-(2-chlorophenyl)methyl isothiocyanate

Base Information

• Chemical Name: bis-(2-chlorophenyl)methyl isothiocyanate
• CAS No.: 439094-21-0
• Molecular Formula: C₁₄H₉Cl₂NS
• Molecular Weight: 294.204
• Mol file: 439094-21-0.mol

Synonyms:bis-(2-chlorophenyl)methyl isothiocyanate

Chemical Property of bis-(2-chlorophenyl)methyl isothiocyanate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bis-(2-chlorophenyl)methyl isothiocyanate

There total 1 articles about bis-(2-chlorophenyl)methyl isothiocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

thiophosgene (463-71-8) + bis-(2-chlorophenyl)methylamine (439094-10-7) → bis-(2-chlorophenyl)methyl isothiocyanate (439094-21-0)

Guidance literature:

With triethylamine; In ethyl acetate; at 0 ℃; for 3.5h;

DOI:10.1021/jm0111088

Reference yield:

bis-(2-chlorophenyl)methyl isothiocyanate (439094-21-0) + (S)-1-(4-Hydrazino-3-nitro-benzenesulfonyl)-pyrrolidine-2-carboxylic acid (439093-26-2) → C25H23Cl2N5O6S2 (439093-47-7)

Guidance literature:

In tetrahydrofuran; at 20 ℃;

DOI:10.1021/jm0111088

upstream raw materials:

thiophosgene

bis-(2-chlorophenyl)methylamine

Downstream raw materials:

C₂₅H₂₃Cl₂N₅O₆S₂