5-Benzyl-2-chloro-10-methyl-8-nitro-5,10-dihydro-3,4,5,10-tetraaza-dibenzo[a,d]cyclohepten-11-one

Base Information

Chemical Name:5-Benzyl-2-chloro-10-methyl-8-nitro-5,10-dihydro-3,4,5,10-tetraaza-dibenzo[a,d]cyclohepten-11-one
CAS No.:189623-83-4
Molecular Formula:C₁₉H₁₄ClN₅O₃
Molecular Weight:395.805
Hs Code.:

Synonyms:5-Benzyl-2-chloro-10-methyl-8-nitro-5,10-dihydro-3,4,5,10-tetraaza-dibenzo[a,d]cyclohepten-11-one

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Chemical Property of 5-Benzyl-2-chloro-10-methyl-8-nitro-5,10-dihydro-3,4,5,10-tetraaza-dibenzo[a,d]cyclohepten-11-one

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Technology Process of 5-Benzyl-2-chloro-10-methyl-8-nitro-5,10-dihydro-3,4,5,10-tetraaza-dibenzo[a,d]cyclohepten-11-one

There total 5 articles about 5-Benzyl-2-chloro-10-methyl-8-nitro-5,10-dihydro-3,4,5,10-tetraaza-dibenzo[a,d]cyclohepten-11-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 189623-72-1
3-Benzylamino-6-chloro-pyridazine-4-carboxylic acid (2-chloro-5-nitro-phenyl)-methyl-amide

: 189623-83-4
5-Benzyl-2-chloro-10-methyl-8-nitro-5,10-dihydro-3,4,5,10-tetraaza-dibenzo[a,d]cyclohepten-11-one

Guidance literature:: With sodium hydride; In 1,4-dioxane; for 6h; Heating;
DOI:10.1002/ardp.19973300108

Reference yield:

: 6283-25-6
H₂NC₆H₃(Cl)NO₂

: 189623-83-4
5-Benzyl-2-chloro-10-methyl-8-nitro-5,10-dihydro-3,4,5,10-tetraaza-dibenzo[a,d]cyclohepten-11-one

Guidance literature:: Multi-step reaction with 4 steps

2: 62 percent / KOH / dimethylsulfoxide / 3 h / Ambient temperature

3: 87 percent / dioxane / 24 h / Ambient temperature

4: 92 percent / NaH / dioxane / 6 h / Heating

With potassium hydroxide; sodium hydride; In 1,4-dioxane; dimethyl sulfoxide;
DOI:10.1002/ardp.19973300108

Reference yield:

: 6531-08-4
3,6-dichloropyridazine-5-carboxylic acid chloride

: 189623-83-4
5-Benzyl-2-chloro-10-methyl-8-nitro-5,10-dihydro-3,4,5,10-tetraaza-dibenzo[a,d]cyclohepten-11-one

Guidance literature:: Multi-step reaction with 4 steps

2: 62 percent / KOH / dimethylsulfoxide / 3 h / Ambient temperature

3: 87 percent / dioxane / 24 h / Ambient temperature

4: 92 percent / NaH / dioxane / 6 h / Heating

With potassium hydroxide; sodium hydride; In 1,4-dioxane; dimethyl sulfoxide;
DOI:10.1002/ardp.19973300108