1-(5-benzyloxy-4-methoxy-2-nitrobenzyl)-7-benzyloxy-6-methoxy-3,4-dihydroisoquinoline methiodide

Base Information

Chemical Name:1-(5-benzyloxy-4-methoxy-2-nitrobenzyl)-7-benzyloxy-6-methoxy-3,4-dihydroisoquinoline methiodide
CAS No.:110674-47-0
Molecular Formula:C₃₃H₃₃N₂O₆*I
Molecular Weight:680.539
Hs Code.:

Synonyms:1-(5-benzyloxy-4-methoxy-2-nitrobenzyl)-7-benzyloxy-6-methoxy-3,4-dihydroisoquinoline methiodide

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Chemical Property of 1-(5-benzyloxy-4-methoxy-2-nitrobenzyl)-7-benzyloxy-6-methoxy-3,4-dihydroisoquinoline methiodide

Chemical Property:

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Technology Process of 1-(5-benzyloxy-4-methoxy-2-nitrobenzyl)-7-benzyloxy-6-methoxy-3,4-dihydroisoquinoline methiodide

There total 1 articles about 1-(5-benzyloxy-4-methoxy-2-nitrobenzyl)-7-benzyloxy-6-methoxy-3,4-dihydroisoquinoline methiodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 116282-35-0
1-(5-benzyloxy-4-methoxy-2-nitrobenzyl)-7-benzyloxy-6-methoxy-3,4-dihydroisoquinoline

: 74-88-4
methyl iodide

: 110674-47-0
1-(5-benzyloxy-4-methoxy-2-nitrobenzyl)-7-benzyloxy-6-methoxy-3,4-dihydroisoquinoline methiodide

Guidance literature:: In chloroform; benzene; Ambient temperature;

Reference yield: 80.0%

: 110674-47-0
1-(5-benzyloxy-4-methoxy-2-nitrobenzyl)-7-benzyloxy-6-methoxy-3,4-dihydroisoquinoline methiodide

: 110674-53-8
1-(5-benzyloxy-4-methoxy-2-nitrobenzyl)-7-benzyloxy-6-methoxy-1,2,3,4-tetrahydro-2-methylisoquinoline

Guidance literature:: With sodium tetrahydroborate; In methanol; for 2h; Ambient temperature;

Reference yield:

: 110674-47-0
1-(5-benzyloxy-4-methoxy-2-nitrobenzyl)-7-benzyloxy-6-methoxy-3,4-dihydroisoquinoline methiodide

: 110674-55-0
1-(2-amino-5-hydroxy-4-methoxybenzyl)-7-hydroxy-6-methoxy-1,2,3,4-tetrahydro-2-methylisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / NaBH₄ / methanol / 2 h / Ambient temperature

2: 65 percent / H₂ / 10percent Pd/C / methanol / 3 h / 2585.7 Torr

With sodium tetrahydroborate; hydrogen; palladium on activated charcoal; In methanol;