methyl 2-<3-<3--N-(3-methylbutyl)carbamoylmethyl>ureido>phenyl>acetate

Base Information

Chemical Name:methyl 2-<3-<3--N-(3-methylbutyl)carbamoylmethyl>ureido>phenyl>acetate
CAS No.:183178-12-3
Molecular Formula:C₃₂H₃₈N₄O₆
Molecular Weight:574.677
Hs Code.:

methyl 2-<3-<3-<N-<2-(N-methyl-N-phenylcarbamoylmethoxy)phenyl>-N-(3-methylbutyl)carbamoylmethyl>ureido>phenyl>acetate

Synonyms:methyl 2-<3-<3--N-(3-methylbutyl)carbamoylmethyl>ureido>phenyl>acetate

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Chemical Property of methyl 2-<3-<3--N-(3-methylbutyl)carbamoylmethyl>ureido>phenyl>acetate

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Technology Process of methyl 2-<3-<3--N-(3-methylbutyl)carbamoylmethyl>ureido>phenyl>acetate

There total 7 articles about methyl 2-<3-<3--N-(3-methylbutyl)carbamoylmethyl>ureido>phenyl>acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 870-63-3
prenyl bromide

: 183178-12-3
methyl 2-<3-<3--N-(3-methylbutyl)carbamoylmethyl>ureido>phenyl>acetate

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) NaH / 1.) THF, 55 deg C, 1.5 h, 2.) THF, RT, overnight

2: 90 percent / H₂ / 5 percent Pd/C / methanol / 3 h / 760 Torr

3: 76 percent / K₂CO₃ / dimethylformamide / 3.5 h / 70 °C

4: 99 percent / TFA / CH₂Cl₂ / 1 h / 0 °C

5: 1.) THF, RT, 10 min, 2.) toluene, reflux, 1 h

With hydrogen; sodium hydride; potassium carbonate; trifluoroacetic acid; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1248/cpb.47.755

Reference yield:

: 183180-09-8
N-(2-benzyloxyphenyl)-2-(N-tert-butoxycarbonylamino)acetamide

: 183178-12-3
methyl 2-<3-<3--N-(3-methylbutyl)carbamoylmethyl>ureido>phenyl>acetate

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) NaH / 1.) THF, 55 deg C, 1.5 h, 2.) THF, RT, overnight

2: 90 percent / H₂ / 5 percent Pd/C / methanol / 3 h / 760 Torr

3: 76 percent / K₂CO₃ / dimethylformamide / 3.5 h / 70 °C

4: 99 percent / TFA / CH₂Cl₂ / 1 h / 0 °C

5: 1.) THF, RT, 10 min, 2.) toluene, reflux, 1 h

With hydrogen; sodium hydride; potassium carbonate; trifluoroacetic acid; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1248/cpb.47.755

Reference yield:

: 237747-77-2
N-(2-benzyloxyphenyl)-N-(3-methyl-2-butenyl)-2-(N-tert-butoxycarbonylamino)acetamide

: 183178-12-3
methyl 2-<3-<3--N-(3-methylbutyl)carbamoylmethyl>ureido>phenyl>acetate

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / H₂ / 5 percent Pd/C / methanol / 3 h / 760 Torr

2: 76 percent / K₂CO₃ / dimethylformamide / 3.5 h / 70 °C

3: 99 percent / TFA / CH₂Cl₂ / 1 h / 0 °C

4: 1.) THF, RT, 10 min, 2.) toluene, reflux, 1 h

With hydrogen; potassium carbonate; trifluoroacetic acid; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1248/cpb.47.755