Technology Process of 4-(2-nitro phenylthio)benzoic acid
There total 3 articles about 4-(2-nitro phenylthio)benzoic acid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 89 percent / sodium ethylate / ethanol / 3 h / Ambient temperature
2: 1.) NBS, benzoyl-peroxide; 2.) silver nitrate / 1.) CCl4, reflux, 15 h; 2.) acetone, water, room temp., 1 h
With
N-Bromosuccinimide; Perbenzoic acid; sodium ethanolate; silver nitrate;
In
ethanol;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 89 percent / sodium ethylate / ethanol / 3 h / Ambient temperature
2: 1.) NBS, benzoyl-peroxide; 2.) silver nitrate / 1.) CCl4, reflux, 15 h; 2.) acetone, water, room temp., 1 h
With
N-Bromosuccinimide; Perbenzoic acid; sodium ethanolate; silver nitrate;
In
ethanol;
- Guidance literature:
-
With
N-Bromosuccinimide; Perbenzoic acid; silver nitrate;
Yield given. Multistep reaction. Yields of byproduct given;
1.) CCl4, reflux, 15 h; 2.) acetone, water, room temp., 1 h;
