methyl (4-methylphenyl 5-amino-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ulopyranoside)onate

Base Information

Chemical Name:methyl (4-methylphenyl 5-amino-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ulopyranoside)onate
CAS No.:1235555-31-3
Molecular Formula:C₁₈H₂₃NO₈S
Molecular Weight:413.449
Hs Code.:

Synonyms:methyl (4-methylphenyl 5-amino-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ulopyranoside)onate

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Chemical Property of methyl (4-methylphenyl 5-amino-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ulopyranoside)onate

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Technology Process of methyl (4-methylphenyl 5-amino-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ulopyranoside)onate

There total 6 articles about methyl (4-methylphenyl 5-amino-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ulopyranoside)onate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: C₁₇H₂₅NO₇S

: 7693-46-1
4-Nitrophenyl chloroformate

: 1235555-31-3
methyl (4-methylphenyl 5-amino-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ulopyranoside)onate

Guidance literature:: With sodium hydrogencarbonate; In water; acetonitrile; at 0 ℃; for 3h;
DOI:10.1002/ejoc.202100718

Reference yield:

: 106-45-6
para-thiocresol

: 1235555-31-3
methyl (4-methylphenyl 5-amino-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ulopyranoside)onate

Guidance literature:: Multi-step reaction with 3 steps

1: boron trifluoride diethyl etherate / dichloromethane / 0 °C / Inert atmosphere

2: methanesulfonic acid / methanol / Reflux

3: sodium hydrogencarbonate / acetonitrile; water / 0 °C

With methanesulfonic acid; boron trifluoride diethyl etherate; sodium hydrogencarbonate; In methanol; dichloromethane; water; acetonitrile;
DOI:10.1016/j.carres.2014.02.006

Reference yield:

: 108740-39-2,6931-68-6,72690-21-2,73208-82-9,108740-37-0,108740-38-1,119241-63-3,119241-64-4,119241-65-5,147129-72-4,147129-73-5,74006-95-4
(1S,2R)-1-((2R,3R,4S,6R)-3-acetamido-4,6-diacetoxy-6-(methoxycarbonyl)tetrahydro-2H-pyran-2-yl)propane-1,2,3-triyl triacetate

: 1235555-31-3
methyl (4-methylphenyl 5-amino-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ulopyranoside)onate

Guidance literature:: Multi-step reaction with 3 steps

1: boron trifluoride diethyl etherate / dichloromethane / 0 °C / Inert atmosphere

2: methanesulfonic acid / methanol / Reflux

3: sodium hydrogencarbonate / acetonitrile; water / 0 °C

With methanesulfonic acid; boron trifluoride diethyl etherate; sodium hydrogencarbonate; In methanol; dichloromethane; water; acetonitrile;
DOI:10.1016/j.carres.2014.02.006