1-(1-(4-((hex-5-ene-1-yloxy)methyl)phenyl)-2-methylpropoxy)-2,2,6,6-tetramethyl piperidine

Base Information

Chemical Name:1-(1-(4-((hex-5-ene-1-yloxy)methyl)phenyl)-2-methylpropoxy)-2,2,6,6-tetramethyl piperidine
CAS No.:1426692-30-9
Molecular Formula:C₂₆H₄₃NO₂
Molecular Weight:401.633
Hs Code.:

Synonyms:1-(1-(4-((hex-5-ene-1-yloxy)methyl)phenyl)-2-methylpropoxy)-2,2,6,6-tetramethyl piperidine

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Chemical Property of 1-(1-(4-((hex-5-ene-1-yloxy)methyl)phenyl)-2-methylpropoxy)-2,2,6,6-tetramethyl piperidine

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Technology Process of 1-(1-(4-((hex-5-ene-1-yloxy)methyl)phenyl)-2-methylpropoxy)-2,2,6,6-tetramethyl piperidine

There total 6 articles about 1-(1-(4-((hex-5-ene-1-yloxy)methyl)phenyl)-2-methylpropoxy)-2,2,6,6-tetramethyl piperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1-[1-(4-iodomethyl-phenyl)-2-methyl-propoxy]-2,2,6,6-tetramethyl-piperidine

: 821-41-0
5-Hexen-1-ol

: 1426692-30-9
1-(1-(4-((hex-5-ene-1-yloxy)methyl)phenyl)-2-methylpropoxy)-2,2,6,6-tetramethyl piperidine

Guidance literature:: 5-Hexen-1-ol; With sodium hydride; In tetrahydrofuran; mineral oil; at 70 ℃; for 2h;

1-[1-(4-iodomethyl-phenyl)-2-methyl-propoxy]-2,2,6,6-tetramethyl-piperidine; at 70 ℃; for 30h;
DOI:10.1002/chem.201200499

Reference yield:

: 4-(1-hydroxy-2-methylpropyl)-benzaldehyde

: 1426692-30-9
1-(1-(4-((hex-5-ene-1-yloxy)methyl)phenyl)-2-methylpropoxy)-2,2,6,6-tetramethyl piperidine

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogen bromide; acetic acid / dichloromethane / 14 h / 0 - 20 °C

2.1: copper; copper(II) bis(trifluoromethanesulfonate); 4,4'-di-tert-butyl-2,2'-bipyridine / benzene / 28 h / 80 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / 20 °C

4.1: sodium iodide; chloro-trimethyl-silane / acetonitrile / 6 h / 20 °C

5.1: sodium hydride / mineral oil; tetrahydrofuran / 2 h / 70 °C

5.2: 30 h / 70 °C

With lithium aluminium tetrahydride; chloro-trimethyl-silane; hydrogen bromide; copper(II) bis(trifluoromethanesulfonate); copper; sodium hydride; acetic acid; 4,4'-di-tert-butyl-2,2'-bipyridine; sodium iodide; In tetrahydrofuran; dichloromethane; acetonitrile; mineral oil; benzene;
DOI:10.1002/chem.201200499

Reference yield:

: 4-[2-methyl-1-(2,2,6,6-tetramethyl-piperidin-1-yloxy)-propyl]-benzaldehyde

: 1426692-30-9
1-(1-(4-((hex-5-ene-1-yloxy)methyl)phenyl)-2-methylpropoxy)-2,2,6,6-tetramethyl piperidine

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / 20 °C

2.1: sodium iodide; chloro-trimethyl-silane / acetonitrile / 6 h / 20 °C

3.1: sodium hydride / mineral oil; tetrahydrofuran / 2 h / 70 °C

3.2: 30 h / 70 °C

With lithium aluminium tetrahydride; chloro-trimethyl-silane; sodium hydride; sodium iodide; In tetrahydrofuran; acetonitrile; mineral oil;
DOI:10.1002/chem.201200499