C₃₇H₄₆O₁₃

Base Information

Chemical Name:C₃₇H₄₆O₁₃
CAS No.:1569902-34-6
Molecular Formula:C₃₇H₄₆O₁₃
Molecular Weight:698.764
Hs Code.:

C<sub>37</sub>H<sub>46</sub>O<sub>13</sub>

Synonyms:C₃₇H₄₆O₁₃

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Chemical Property of C₃₇H₄₆O₁₃

Chemical Property:

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Technology Process of C₃₇H₄₆O₁₃

There total 11 articles about C₃₇H₄₆O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1569902-23-3
methyl 2,4,6-tri-O-benzyl-3-O-[methyl (4,5:7,8-di-O-isopropylidene-3-deoxy-β-D-manno-2-octulopyranosyl)onate]-β-D-glactopyranoside

: 1569902-34-6
C₃₇H₄₆O₁₃

Guidance literature:: With toluene-4-sulfonic acid; In methanol; at 0 - 20 ℃; for 10h;
DOI:10.1021/ol500275j

Reference yield:

: 1569902-22-2
methyl 2,4,6-tri-O-benzyl-3-O-[methyl (4,5:7,8-di-O-isopropylidene-3-deoxy-3-iodo-D-glycero-β-D-galacto-2-octulopyranosyl)onate]-β-D-glactopyranoside

: 1569902-34-6
C₃₇H₄₆O₁₃

Guidance literature:: Multi-step reaction with 2 steps

1: 2,2'-azobis(isobutyronitrile); triphenylstannane / toluene / 1 h / 120 °C

2: toluene-4-sulfonic acid / methanol / 10 h / 0 - 20 °C

With 2,2'-azobis(isobutyronitrile); triphenylstannane; toluene-4-sulfonic acid; In methanol; toluene;
DOI:10.1021/ol500275j

Reference yield:

: 31024-99-4,54187-72-3,76249-79-1
1,2-dideoxy-4,5:7,8-di-O-isopropylidene-D-erythro-D-manno-1-yno-octitol

: 1569902-34-6
C₃₇H₄₆O₁₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

1.2: 1 h / 20 °C / Inert atmosphere

2.1: N-Bromosuccinimide; silver nitrate / acetone / 0.5 h / 0 - 20 °C

3.1: magnesium sulfate; sodium hydrogencarbonate / water / 0.5 h / 20 °C

3.2: 4 h / 0 °C

4.1: palladium 10% on activated carbon; hydrogen / methanol; ethyl acetate / 10 h

5.1: dmap / acetonitrile / 0 °C

6.1: triethyl phosphite / 2.5 h / 120 °C

7.1: N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate / dichloromethane; acetonitrile / 3 h / -45 °C / Molecular sieve

8.1: 2,2'-azobis(isobutyronitrile); triphenylstannane / toluene / 1 h / 120 °C

9.1: toluene-4-sulfonic acid / methanol / 10 h / 0 - 20 °C

With dmap; N-Bromosuccinimide; N-iodo-succinimide; 2,2'-azobis(isobutyronitrile); trimethylsilyl trifluoromethanesulfonate; palladium 10% on activated carbon; triphenylstannane; hydrogen; sodium hydride; sodium hydrogencarbonate; magnesium sulfate; toluene-4-sulfonic acid; silver nitrate; triethyl phosphite; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; acetone; toluene; acetonitrile; mineral oil;
DOI:10.1021/ol500275j