C₁₃H₁₇⁽²⁾H₂NO₂S

Base Information

Chemical Name:C₁₃H₁₇⁽²⁾H₂NO₂S
CAS No.:1265228-77-0
Molecular Formula:C₁₃H₁₉NO₂S
Molecular Weight:255.349
Hs Code.:

C<sub>13</sub>H<sub>17</sub><sup>(2)</sup>H<sub>2</sub>NO<sub>2</sub>S

Synonyms:C₁₃H₁₇⁽²⁾H₂NO₂S

Suppliers and Price of C₁₃H₁₇⁽²⁾H₂NO₂S

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of C₁₃H₁₇⁽²⁾H₂NO₂S

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of C₁₃H₁₇⁽²⁾H₂NO₂S

There total 7 articles about C₁₃H₁₇⁽²⁾H₂NO₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: C₁₀H₁₈⁽²⁾H₂O₃S

: 70-55-3
toluene-4-sulfonamide

: 1265228-77-0
C₁₃H₁₇⁽²⁾H₂NO₂S

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃;
DOI:10.1021/jo102338a

Reference yield:

: 147753-81-9
C₁₂H₂₀O₄

: 1265228-77-0
C₁₃H₁₇⁽²⁾H₂NO₂S

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium aluminium deuteride / diethyl ether / -20 - 0 °C / Inert atmosphere

2.1: methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C

3.1: lithium aluminium tetrahydride / diethyl ether / 2 h / Inert atmosphere; Reflux

4.1: toluene-4-sulfonic acid / methanol / 1 h

4.2: 20 °C

5.1: potassium carbonate / N,N-dimethyl-formamide / 60 °C

With lithium aluminium tetrahydride; lithium aluminium deuteride; potassium carbonate; toluene-4-sulfonic acid; methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine; In methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo102338a

Reference yield:

: 1265228-94-1
C₁₁H₁₈⁽²⁾H₂O₃

: 1265228-77-0
C₁₃H₁₇⁽²⁾H₂NO₂S

Guidance literature:: Multi-step reaction with 4 steps

1.1: methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C

2.1: lithium aluminium tetrahydride / diethyl ether / 2 h / Inert atmosphere; Reflux

3.1: toluene-4-sulfonic acid / methanol / 1 h

3.2: 20 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 60 °C

With lithium aluminium tetrahydride; potassium carbonate; toluene-4-sulfonic acid; methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine; In methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo102338a