(1S,2S,5S)-(-)-6,6-dimethylbicyclo<3.1.1>heptan-2-yl dimethylphenylsilyl thioketone

Base Information

Chemical Name:(1S,2S,5S)-(-)-6,6-dimethylbicyclo<3.1.1>heptan-2-yl dimethylphenylsilyl thioketone
CAS No.:150615-00-2
Molecular Formula:C₁₈H₂₆SSi
Molecular Weight:302.556
Hs Code.:

Synonyms:(1S,2S,5S)-(-)-6,6-dimethylbicyclo<3.1.1>heptan-2-yl dimethylphenylsilyl thioketone

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Chemical Property of (1S,2S,5S)-(-)-6,6-dimethylbicyclo<3.1.1>heptan-2-yl dimethylphenylsilyl thioketone

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Technology Process of (1S,2S,5S)-(-)-6,6-dimethylbicyclo<3.1.1>heptan-2-yl dimethylphenylsilyl thioketone

There total 4 articles about (1S,2S,5S)-(-)-6,6-dimethylbicyclo<3.1.1>heptan-2-yl dimethylphenylsilyl thioketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 150614-93-0
(1S,2S,5S)-(+)-6,6-dimethylbicyclo[3.1.1]heptan-2-yl dimethylphenylsilyl ketone

: 150615-00-2
(1S,2S,5S)-(-)-6,6-dimethylbicyclo<3.1.1>heptan-2-yl dimethylphenylsilyl thioketone

Guidance literature:: With hydrogenchloride; hydrogen sulfide; In diethyl ether; at -30 ℃;

Reference yield: 45.0%

: 150614-94-1
(1S,2R,5S)-(-)-6,6-dimethylbicyclo<3.1.1>heptan-2-yl dimethylphenylsilyl ketone

: 150615-00-2
(1S,2S,5S)-(-)-6,6-dimethylbicyclo<3.1.1>heptan-2-yl dimethylphenylsilyl thioketone

Guidance literature:: With hydrogenchloride; hydrogen sulfide; In diethyl ether; at -30 ℃;

Reference yield:

: 108318-82-7,150614-86-1
myrtanyl chloride

: 150615-00-2
(1S,2S,5S)-(-)-6,6-dimethylbicyclo<3.1.1>heptan-2-yl dimethylphenylsilyl thioketone

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 1.) -78 deg C, 1 h, 2.) 0 deg C, 30 min

2: 77 percent / HCl, H₂S / diethyl ether / -30 °C

With hydrogenchloride; hydrogen sulfide; In tetrahydrofuran; diethyl ether;