(E)-(phenylthio)ethenyl methyl selenide

Base Information

• Chemical Name: (E)-(phenylthio)ethenyl methyl selenide
• CAS No.: 95391-84-7
• Molecular Formula: C₉H₁₀SSe
• Molecular Weight: 229.204
• Mol file: 95391-84-7.mol

Synonyms:(E)-(phenylthio)ethenyl methyl selenide

Chemical Property of (E)-(phenylthio)ethenyl methyl selenide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (E)-(phenylthio)ethenyl methyl selenide

There total 3 articles about (E)-(phenylthio)ethenyl methyl selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

(E)-2-chlorovinylthiobenzene (26620-11-1) + lithium methyl selenide (50491-55-9) → (E)-(phenylthio)ethenyl methyl selenide (95391-84-7)

Guidance literature:

In N,N,N,N,N,N-hexamethylphosphoric triamide; at 25 ℃; for 1h;

DOI:10.1016/S0040-4039(01)91274-2

Reference yield:

lithium methyl selenide (50491-55-9) → (E)-(phenylthio)ethenyl methyl selenide (95391-84-7)

Guidance literature:

In tetrahydrofuran; N,N-dimethyl-formamide; at 100 ℃;

DOI:10.1016/S0040-4020(01)87301-4

Reference yield:

benzenesulfenyl chloride (931-59-9) → (E)-(phenylthio)ethenyl methyl selenide (95391-84-7)

Guidance literature:

Multi-step reaction with 2 steps

2: 85 percent / hexamethylphosphoric acid triamide / 1 h / 25 °C

In N,N,N,N,N,N-hexamethylphosphoric triamide;

DOI:10.1016/S0040-4039(01)91274-2

upstream raw materials:

(E)-2-chlorovinylthiobenzene

lithium methyl selenide

benzenesulfenyl chloride

Downstream raw materials:

biphenyl

(E)-[2-(phenylsulfanyl)vinyl]benzene

(E)-2-phenylthio-1-ethenyl diselenide

(E)-2-phenylthio-1-ethenyl acetyl selenide