1-Hydroxy-5,9-bis-(toluene-4-sulfonyl)-1,5,9-triaza-cyclododecane-2-carbonitrile

Base Information

Chemical Name:1-Hydroxy-5,9-bis-(toluene-4-sulfonyl)-1,5,9-triaza-cyclododecane-2-carbonitrile
CAS No.:174192-36-0
Molecular Formula:C₂₄H₃₂N₄O₅S₂
Molecular Weight:520.674
Hs Code.:

Synonyms:1-Hydroxy-5,9-bis-(toluene-4-sulfonyl)-1,5,9-triaza-cyclododecane-2-carbonitrile

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Chemical Property of 1-Hydroxy-5,9-bis-(toluene-4-sulfonyl)-1,5,9-triaza-cyclododecane-2-carbonitrile

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Technology Process of 1-Hydroxy-5,9-bis-(toluene-4-sulfonyl)-1,5,9-triaza-cyclododecane-2-carbonitrile

There total 3 articles about 1-Hydroxy-5,9-bis-(toluene-4-sulfonyl)-1,5,9-triaza-cyclododecane-2-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 294-80-4
1,5,9-triazacyclododecane

: 174192-36-0
1-Hydroxy-5,9-bis-(toluene-4-sulfonyl)-1,5,9-triaza-cyclododecane-2-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / NaOH / H₂O; diethyl ether / 1 h / 0 °C

2: 1.) Na₂WO₄*2H₂O, 30percent H₂O₂, 2.) 4N HCl / 1.) THF, H₂O, 25 deg C, 18 h, 2.) H₂O, 25 deg C, 30 h

With hydrogenchloride; sodium hydroxide; sodium tungstate; dihydrogen peroxide; In diethyl ether; water;
DOI:10.1021/jo951637h

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 174192-36-0
1-Hydroxy-5,9-bis-(toluene-4-sulfonyl)-1,5,9-triaza-cyclododecane-2-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / NaOH / H₂O; diethyl ether / 1 h / 0 °C

2: 1.) Na₂WO₄*2H₂O, 30percent H₂O₂, 2.) 4N HCl / 1.) THF, H₂O, 25 deg C, 18 h, 2.) H₂O, 25 deg C, 30 h

With hydrogenchloride; sodium hydroxide; sodium tungstate; dihydrogen peroxide; In diethyl ether; water;
DOI:10.1021/jo951637h

Reference yield:

: 151-50-8
potassium cyanide

: 164913-31-9
N¹,N⁵-ditosyl-1,5,9-triazacyclododecane

: 174192-36-0
1-Hydroxy-5,9-bis-(toluene-4-sulfonyl)-1,5,9-triaza-cyclododecane-2-carbonitrile

Guidance literature:: With hydrogenchloride; sodium tungstate; dihydrogen peroxide; Yield given. Multistep reaction; 1.) THF, H₂O, 25 deg C, 18 h, 2.) H₂O, 25 deg C, 30 h;
DOI:10.1021/jo951637h