N-((4-(diphenylphosphino)-1-(4-ethoxyphenyl)-2,5-dimethyl-1H-pyrrol-3-yl)methylene)-1-phenylethanamine

Base Information

Chemical Name:N-((4-(diphenylphosphino)-1-(4-ethoxyphenyl)-2,5-dimethyl-1H-pyrrol-3-yl)methylene)-1-phenylethanamine
CAS No.:1429309-05-6
Molecular Formula:C₃₅H₃₅N₂OP
Molecular Weight:530.649
Hs Code.:

Synonyms:N-((4-(diphenylphosphino)-1-(4-ethoxyphenyl)-2,5-dimethyl-1H-pyrrol-3-yl)methylene)-1-phenylethanamine

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Chemical Property of N-((4-(diphenylphosphino)-1-(4-ethoxyphenyl)-2,5-dimethyl-1H-pyrrol-3-yl)methylene)-1-phenylethanamine

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Technology Process of N-((4-(diphenylphosphino)-1-(4-ethoxyphenyl)-2,5-dimethyl-1H-pyrrol-3-yl)methylene)-1-phenylethanamine

There total 8 articles about N-((4-(diphenylphosphino)-1-(4-ethoxyphenyl)-2,5-dimethyl-1H-pyrrol-3-yl)methylene)-1-phenylethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1429309-04-5
N-((4-(diphenylphosphoryl)-1-(4-ethoxyphenyl)-2,5-dimethyl-1H-pyrrol-3-yl)methylene)-1-phenylethanamine

: 1429309-05-6
N-((4-(diphenylphosphino)-1-(4-ethoxyphenyl)-2,5-dimethyl-1H-pyrrol-3-yl)methylene)-1-phenylethanamine

Guidance literature:: With trichlorosilane; triethylamine; In toluene; at 120 ℃; for 6h; Sealed tube;
DOI:10.1002/hc.21069

Reference yield:

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 1429309-05-6
N-((4-(diphenylphosphino)-1-(4-ethoxyphenyl)-2,5-dimethyl-1H-pyrrol-3-yl)methylene)-1-phenylethanamine

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 120 h / 20 °C

2: trichlorophosphate / 2 h / 20 °C

3: methanol / 4 h / Reflux

4: triethylamine; trichlorosilane / toluene / 6 h / 120 °C / Sealed tube

With trichlorosilane; triethylamine; trichlorophosphate; In pyridine; methanol; toluene; 2: |Vilsmeier Reaction;
DOI:10.1002/hc.21069

Reference yield:

: 54609-18-6
1-(4-ethoxyphenyl)-2,5-dimethyl-1H-pyrrole

: 1429309-05-6
N-((4-(diphenylphosphino)-1-(4-ethoxyphenyl)-2,5-dimethyl-1H-pyrrol-3-yl)methylene)-1-phenylethanamine

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 120 h / 20 °C

2: trichlorophosphate / 2 h / 20 °C

3: methanol / 4 h / Reflux

4: triethylamine; trichlorosilane / toluene / 6 h / 120 °C / Sealed tube

With trichlorosilane; triethylamine; trichlorophosphate; In pyridine; methanol; toluene; 2: |Vilsmeier Reaction;
DOI:10.1002/hc.21069