3-(tert-Butyl-dimethyl-silanyloxymethyl)-6-[2-(tert-butyl-dimethyl-silanyloxy)-phenoxymethyl]-[1,2]dithiine

Base Information

Chemical Name:3-(tert-Butyl-dimethyl-silanyloxymethyl)-6-[2-(tert-butyl-dimethyl-silanyloxy)-phenoxymethyl]-[1,2]dithiine
CAS No.:172832-31-4
Molecular Formula:C₂₄H₄₀O₃S₂Si₂
Molecular Weight:496.883
Hs Code.:

Synonyms:3-(tert-Butyl-dimethyl-silanyloxymethyl)-6-[2-(tert-butyl-dimethyl-silanyloxy)-phenoxymethyl]-[1,2]dithiine

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Chemical Property of 3-(tert-Butyl-dimethyl-silanyloxymethyl)-6-[2-(tert-butyl-dimethyl-silanyloxy)-phenoxymethyl]-[1,2]dithiine

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Technology Process of 3-(tert-Butyl-dimethyl-silanyloxymethyl)-6-[2-(tert-butyl-dimethyl-silanyloxy)-phenoxymethyl]-[1,2]dithiine

There total 6 articles about 3-(tert-Butyl-dimethyl-silanyloxymethyl)-6-[2-(tert-butyl-dimethyl-silanyloxy)-phenoxymethyl]-[1,2]dithiine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.3%

: 80180-46-7
1-<(tert-butyldimethylsilyl)oxy>-2-hydroxybenzene

: 165404-83-1
3-[(tert-butyldimethylsilyloxy)methyl]-6-(hydroxymethyl)-1,2-dithiin

: 172832-31-4
3-(tert-Butyl-dimethyl-silanyloxymethyl)-6-[2-(tert-butyl-dimethyl-silanyloxy)-phenoxymethyl]-[1,2]dithiine

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 5 ℃; for 3h;
DOI:10.1021/jm00014a016

Reference yield:

: 120-80-9,19481-10-8,37349-32-9
benzene-1,2-diol

: 172832-31-4
3-(tert-Butyl-dimethyl-silanyloxymethyl)-6-[2-(tert-butyl-dimethyl-silanyloxy)-phenoxymethyl]-[1,2]dithiine

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / imidazole / dimethylformamide / 3 h

2: 62.3 percent / triphenylphosphine, diethyl azodicarboxylate / tetrahydrofuran / 3 h / 5 °C

With 1H-imidazole; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm00014a016

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 172832-31-4
3-(tert-Butyl-dimethyl-silanyloxymethyl)-6-[2-(tert-butyl-dimethyl-silanyloxy)-phenoxymethyl]-[1,2]dithiine

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / imidazole / dimethylformamide / 3 h

2: 62.3 percent / triphenylphosphine, diethyl azodicarboxylate / tetrahydrofuran / 3 h / 5 °C

With 1H-imidazole; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm00014a016