(R)-1-(2-(1-(tert-butyldimethylsilyloxy)-2-methylpropan-2-yl)-1,3-dithian-2-yl)-4-(4-methoxybenzyloxy)butan-2-ol

Base Information

• Chemical Name: (R)-1-(2-(1-(tert-butyldimethylsilyloxy)-2-methylpropan-2-yl)-1,3-dithian-2-yl)-4-(4-methoxybenzyloxy)butan-2-ol
• CAS No.: 1211323-85-1
• Molecular Formula: C₂₆H₄₆O₄S₂Si
• Molecular Weight: 514.866

Synonyms:(R)-1-(2-(1-(tert-butyldimethylsilyloxy)-2-methylpropan-2-yl)-1,3-dithian-2-yl)-4-(4-methoxybenzyloxy)butan-2-ol

Chemical Property of (R)-1-(2-(1-(tert-butyldimethylsilyloxy)-2-methylpropan-2-yl)-1,3-dithian-2-yl)-4-(4-methoxybenzyloxy)butan-2-ol

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of (R)-1-(2-(1-(tert-butyldimethylsilyloxy)-2-methylpropan-2-yl)-1,3-dithian-2-yl)-4-(4-methoxybenzyloxy)butan-2-ol

There total 1 articles about (R)-1-(2-(1-(tert-butyldimethylsilyloxy)-2-methylpropan-2-yl)-1,3-dithian-2-yl)-4-(4-methoxybenzyloxy)butan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

(2-(1,3-dithian-2-yl)-2-methylpropoxy)(tert-butyl)dimethylsilane (254893-76-0) + (R)-2-(2-((4-methoxybenzyl)oxy)ethyl)oxirane (195257-62-6) → (R)-1-(2-(1-(tert-butyldimethylsilyloxy)-2-methylpropan-2-yl)-1,3-dithian-2-yl)-4-(4-methoxybenzyloxy)butan-2-ol (1211323-85-1)

Guidance literature:

(2-(1,3-dithian-2-yl)-2-methylpropoxy)(tert-butyl)dimethylsilane; With n-butyllithium; In tetrahydrofuran; hexane; at 20 - 35 ℃; for 0.416667h; Inert atmosphere;

(R)-2-(2-((4-methoxybenzyl)oxy)ethyl)oxirane; In tetrahydrofuran; hexane; at 20 ℃; Inert atmosphere;

DOI:10.1021/ol100123p

Reference yield: 94.0%

(R)-1-(2-(1-(tert-butyldimethylsilyloxy)-2-methylpropan-2-yl)-1,3-dithian-2-yl)-4-(4-methoxybenzyloxy)butan-2-ol (1211323-85-1) + methyl iodide (74-88-4) → (R)-tert-butyl(2-(2-(2-methoxy-4-(4-methoxybenzyloxy)butyl)-1,3-dithian-2-yl)-2-methylpropoxy)dimethylsilane (1211323-56-6)

Guidance literature:

With 15-crown-5; sodium hydride; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/ol100123p

upstream raw materials:

(2-(1,3-dithian-2-yl)-2-methylpropoxy)(tert-butyl)dimethylsilane

(R)-2-(2-((4-methoxybenzyl)oxy)ethyl)oxirane

Downstream raw materials:

(R)-tert-butyl(2-(2-(2-methoxy-4-(4-methoxybenzyloxy)butyl)-1,3-dithian-2-yl)-2-methylpropoxy)dimethylsilane

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