methyl 4-(methylsulfonyl)-6-oxo-2-phenyl-1,6-dihydro-5-pyrimidinecarboxylate

Base Information

Chemical Name:methyl 4-(methylsulfonyl)-6-oxo-2-phenyl-1,6-dihydro-5-pyrimidinecarboxylate
CAS No.:118996-57-9
Molecular Formula:C₁₃H₁₂N₂O₅S
Molecular Weight:308.315
Hs Code.:
Mol file:118996-57-9.mol

Synonyms:methyl 2-phenyl-4-methylsulfonyl-6-oxopyrimidine-5-carboxylate

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Chemical Property of methyl 4-(methylsulfonyl)-6-oxo-2-phenyl-1,6-dihydro-5-pyrimidinecarboxylate

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Technology Process of methyl 4-(methylsulfonyl)-6-oxo-2-phenyl-1,6-dihydro-5-pyrimidinecarboxylate

There total 6 articles about methyl 4-(methylsulfonyl)-6-oxo-2-phenyl-1,6-dihydro-5-pyrimidinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 87693-90-1
methyl 3,4-dihydro-4-methylthio-2-phenyl-4-oxopyrimidine-5-carboxylate

: 118996-57-9
methyl 2-phenyl-4-methylsulfonyl-6-oxopyrimidine-5-carboxylate

Guidance literature:: With dihydrogen peroxide; In acetic acid; at 60 ℃; for 6h;

Reference yield:

: 19607-08-0
methyl 2-methoxycarbonyl-3,3-di(methylsulfanyl)acrylate

: 118996-57-9
methyl 2-phenyl-4-methylsulfonyl-6-oxopyrimidine-5-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / 1.)K₂CO₃; 2.) 10percent HCl / dimethylsulfoxide / 10 h / 100 °C

2: 70 percent / 30percent H₂O₂ / acetic acid / 6 h / 60 °C

With hydrogenchloride; dihydrogen peroxide; potassium carbonate; In acetic acid; dimethyl sulfoxide;

Reference yield:

: 1670-14-0
benzamidine monohydrochloride

: 118996-57-9
methyl 2-phenyl-4-methylsulfonyl-6-oxopyrimidine-5-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / 1.)K₂CO₃; 2.) 10percent HCl / dimethylsulfoxide / 10 h / 100 °C

2: 70 percent / 30percent H₂O₂ / acetic acid / 6 h / 60 °C

With hydrogenchloride; dihydrogen peroxide; potassium carbonate; In acetic acid; dimethyl sulfoxide;