(2',3',4',6'-tetra-O-acetyl-S-β-D-ribofuranosyl)-5-(p-ethoxyphenyl)-1,2,4-triazole sulfone

Base Information

Chemical Name:(2',3',4',6'-tetra-O-acetyl-S-β-D-ribofuranosyl)-5-(p-ethoxyphenyl)-1,2,4-triazole sulfone
CAS No.:1254105-66-2
Molecular Formula:C₂₁H₂₅N₃O₁₀S
Molecular Weight:511.51
Hs Code.:

Synonyms:(2',3',4',6'-tetra-O-acetyl-S-β-D-ribofuranosyl)-5-(p-ethoxyphenyl)-1,2,4-triazole sulfone

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Chemical Property of (2',3',4',6'-tetra-O-acetyl-S-β-D-ribofuranosyl)-5-(p-ethoxyphenyl)-1,2,4-triazole sulfone

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Technology Process of (2',3',4',6'-tetra-O-acetyl-S-β-D-ribofuranosyl)-5-(p-ethoxyphenyl)-1,2,4-triazole sulfone

There total 5 articles about (2',3',4',6'-tetra-O-acetyl-S-β-D-ribofuranosyl)-5-(p-ethoxyphenyl)-1,2,4-triazole sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1204824-67-8
S-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)-3-mercapto-5-(p-ethoxyphenyl)-1,2,4-triazole

: 1254105-66-2
(2',3',4',6'-tetra-O-acetyl-S-β-D-ribofuranosyl)-5-(p-ethoxyphenyl)-1,2,4-triazole sulfone

Guidance literature:: With potassium permanganate; copper(ll) sulfate pentahydrate; In water; acetonitrile; at 20 ℃;

Reference yield:

: 3-mercapto-5-(p-ethoxyphenyl)-1,2,4-triazole

: 1254105-66-2
(2',3',4',6'-tetra-O-acetyl-S-β-D-ribofuranosyl)-5-(p-ethoxyphenyl)-1,2,4-triazole sulfone

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C / Inert atmosphere

2: potassium permanganate; copper(ll) sulfate pentahydrate / water; acetonitrile / 20 °C

With potassium permanganate; copper(ll) sulfate pentahydrate; boron trifluoride diethyl etherate; In dichloromethane; water; acetonitrile;

Reference yield:

: 94267-66-0
N₂-(4-ethoxybenzoyl)thiosemicarbazide

: 1254105-66-2
(2',3',4',6'-tetra-O-acetyl-S-β-D-ribofuranosyl)-5-(p-ethoxyphenyl)-1,2,4-triazole sulfone

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / ethanol / 78 °C

2: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C / Inert atmosphere

3: potassium permanganate; copper(ll) sulfate pentahydrate / water; acetonitrile / 20 °C

With potassium permanganate; copper(ll) sulfate pentahydrate; boron trifluoride diethyl etherate; sodium hydroxide; In ethanol; dichloromethane; water; acetonitrile;