S-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)-3-mercapto-5-(p-ethoxyphenyl)-1,2,4-triazole

Base Information

Chemical Name:S-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)-3-mercapto-5-(p-ethoxyphenyl)-1,2,4-triazole
CAS No.:1204824-67-8
Molecular Formula:C₂₁H₂₅N₃O₈S
Molecular Weight:479.511
Hs Code.:

Synonyms:S-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)-3-mercapto-5-(p-ethoxyphenyl)-1,2,4-triazole

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Chemical Property of S-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)-3-mercapto-5-(p-ethoxyphenyl)-1,2,4-triazole

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Technology Process of S-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)-3-mercapto-5-(p-ethoxyphenyl)-1,2,4-triazole

There total 4 articles about S-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)-3-mercapto-5-(p-ethoxyphenyl)-1,2,4-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 3-mercapto-5-(p-ethoxyphenyl)-1,2,4-triazole

: 13035-61-5
1,2,3,5-tetraacetylribose

: 1204824-67-8
S-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)-3-mercapto-5-(p-ethoxyphenyl)-1,2,4-triazole

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

Reference yield:

: 94267-66-0
N₂-(4-ethoxybenzoyl)thiosemicarbazide

: 1204824-67-8
S-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)-3-mercapto-5-(p-ethoxyphenyl)-1,2,4-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / ethanol / 78 °C

2: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C / Inert atmosphere

With boron trifluoride diethyl etherate; sodium hydroxide; In ethanol; dichloromethane;

Reference yield:

: 619-86-3
4-(ethoxy)benzoic acid

: 1204824-67-8
S-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)-3-mercapto-5-(p-ethoxyphenyl)-1,2,4-triazole

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuryl dichloride / tetrachloromethane / 50 °C

2: tetrachloromethane / 20 °C

3: sodium hydroxide / ethanol / 78 °C

4: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C / Inert atmosphere

With sulfuryl dichloride; boron trifluoride diethyl etherate; sodium hydroxide; In tetrachloromethane; ethanol; dichloromethane;