5-(N-benzylamino)-2-pentanone ethylene acetal

Base Information

• Chemical Name: 5-(N-benzylamino)-2-pentanone ethylene acetal
• CAS No.: 501346-84-5
• Molecular Formula: C₁₄H₂₁NO₂
• Molecular Weight: 235.326
• Mol file: 501346-84-5.mol

Synonyms:5-(N-benzylamino)-2-pentanone ethylene acetal

Chemical Property of 5-(N-benzylamino)-2-pentanone ethylene acetal

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-(N-benzylamino)-2-pentanone ethylene acetal

There total 1 articles about 5-(N-benzylamino)-2-pentanone ethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

5-iodo-2-pentanone ethylene ketal (3695-28-1) + benzylamine (100-46-9) → 5-(N-benzylamino)-2-pentanone ethylene acetal (501346-84-5)

Guidance literature:

With potassium carbonate; at 70 ℃; for 24h;

DOI:10.1021/ja029114w

Reference yield: 75.0%

5-(N-benzylamino)-2-pentanone ethylene acetal (501346-84-5) + 1-Bromo-2-bromomethyl-benzene (3433-80-5) → 2-[N-benzyl-N-(2-bromobenzyl)amino]-2-pentanone (501346-90-3)

Guidance literature:

5-(N-benzylamino)-2-pentanone ethylene acetal; 1-Bromo-2-bromomethyl-benzene; With potassium carbonate; lithium iodide; In acetonitrile; at 65 ℃; for 24h;

With hydrogenchloride; In tetrahydrofuran; at 20 ℃; for 24h; Further stages.;

DOI:10.1021/ja029114w

Reference yield: 67.0%

2-bromoallyl bromide (513-31-5) + 5-(N-benzylamino)-2-pentanone ethylene acetal (501346-84-5) → 5-[N-benzyl-N-(2-bromoallyl)amino]-2-pentanone ethylene acetal

Guidance literature:

With potassium carbonate; In acetonitrile; at 60 ℃; for 24h;

DOI:10.1021/jo034299q

upstream raw materials:

5-iodo-2-pentanone ethylene ketal

benzylamine

Downstream raw materials:

2-[N-benzyl-N-(2-bromobenzyl)amino]-2-pentanone

5-[N-benzyl-N-(2-bromoallyl)amino]-2-pentanone