1-((3S,4R,5R,6S)-4,5,6-tri(benzyloxy)octa-1,7-dien-3-yl)-4-fluorobenzene

Base Information

Chemical Name:1-((3S,4R,5R,6S)-4,5,6-tri(benzyloxy)octa-1,7-dien-3-yl)-4-fluorobenzene
CAS No.:906098-31-5
Molecular Formula:C₃₅H₃₅FO₃
Molecular Weight:522.66
Hs Code.:

Synonyms:1-((3S,4R,5R,6S)-4,5,6-tri(benzyloxy)octa-1,7-dien-3-yl)-4-fluorobenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-((3S,4R,5R,6S)-4,5,6-tri(benzyloxy)octa-1,7-dien-3-yl)-4-fluorobenzene

Chemical Property:

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Technology Process of 1-((3S,4R,5R,6S)-4,5,6-tri(benzyloxy)octa-1,7-dien-3-yl)-4-fluorobenzene

There total 10 articles about 1-((3S,4R,5R,6S)-4,5,6-tri(benzyloxy)octa-1,7-dien-3-yl)-4-fluorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₁H₄₀FNO₅Se

: 906098-31-5
1-((3S,4R,5R,6S)-4,5,6-tri(benzyloxy)octa-1,7-dien-3-yl)-4-fluorobenzene

Guidance literature:: With dihydrogen peroxide; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/jo0607562

Reference yield:

: 906098-28-0
(3S,4R,5R,6S)-3-(4-fluorophenyl)-4,5,6-tri(benzyloxy)-7-octen-1-ol

: 906098-31-5
1-((3S,4R,5R,6S)-4,5,6-tri(benzyloxy)octa-1,7-dien-3-yl)-4-fluorobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: Bu₃P / tetrahydrofuran

2: aq. H₂O₂ / tetrahydrofuran / 20 °C

With tributylphosphine; dihydrogen peroxide; In tetrahydrofuran;
DOI:10.1021/jo0607562

Reference yield:

: 906098-25-7
methyl (3S,4R,5R,6S)-3-(4-fluorophenyl)-4,5,6-tri(benzyloxy)-7-octenoate

: 906098-31-5
1-((3S,4R,5R,6S)-4,5,6-tri(benzyloxy)octa-1,7-dien-3-yl)-4-fluorobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: LiAlH₄ / diethyl ether / 3 h / 0 - 20 °C

2: Bu₃P / tetrahydrofuran

3: aq. H₂O₂ / tetrahydrofuran / 20 °C

With lithium aluminium tetrahydride; tributylphosphine; dihydrogen peroxide; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo0607562