{[1-(3-Methoxy-phenyl)-meth-(E)-ylidene]-amino}-phenyl-acetic acid methyl ester

Base Information

Chemical Name:{[1-(3-Methoxy-phenyl)-meth-(E)-ylidene]-amino}-phenyl-acetic acid methyl ester
CAS No.:83529-46-8
Molecular Formula:C₁₇H₁₇NO₃
Molecular Weight:283.327
Hs Code.:

Synonyms:{[1-(3-Methoxy-phenyl)-meth-(E)-ylidene]-amino}-phenyl-acetic acid methyl ester

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Chemical Property of {[1-(3-Methoxy-phenyl)-meth-(E)-ylidene]-amino}-phenyl-acetic acid methyl ester

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Technology Process of {[1-(3-Methoxy-phenyl)-meth-(E)-ylidene]-amino}-phenyl-acetic acid methyl ester

There total 3 articles about {[1-(3-Methoxy-phenyl)-meth-(E)-ylidene]-amino}-phenyl-acetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 15028-40-7,13226-98-7
DL-2-phenylglycine methyl ester hydrochloride

: 591-31-1
3-methoxy-benzaldehyde

: 83529-46-8
{[1-(3-Methoxy-phenyl)-meth-(E)-ylidene]-amino}-phenyl-acetic acid methyl ester

Guidance literature:: With magnesium sulfate; triethylamine; In dichloromethane; for 4h; Ambient temperature;

Reference yield:

: 591-31-1
3-methoxy-benzaldehyde

: 24461-61-8,26682-99-5,37760-98-8,6591-61-3
phenylglycine methyl ester

: 83529-46-8
{[1-(3-Methoxy-phenyl)-meth-(E)-ylidene]-amino}-phenyl-acetic acid methyl ester

Guidance literature:: phenylglycine methyl ester; With magnesium sulfate; In dichloromethane; at 20 ℃; for 0.333333h; Inert atmosphere;

3-methoxy-benzaldehyde; With triethylamine; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.tet.2016.07.046

Reference yield:

: 2835-06-5
phenylglycin

: 83529-46-8
{[1-(3-Methoxy-phenyl)-meth-(E)-ylidene]-amino}-phenyl-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / SOCl₂ / 2 h at 45 deg C, 2 h at room temp.

2: 56 percent / Et₃N, MgSO₄ / CH₂Cl₂ / 4 h / Ambient temperature

With thionyl chloride; magnesium sulfate; triethylamine; In dichloromethane;