N-(2,6-diisopropylphenyl)-1,6-bis[4-(1,1,3,3-tetramethylbutyl)phenoxy]-11-iodoterrylene-3,4-dicarboximide

Base Information

• Chemical Name: N-(2,6-diisopropylphenyl)-1,6-bis[4-(1,1,3,3-tetramethylbutyl)phenoxy]-11-iodoterrylene-3,4-dicarboximide
• CAS No.: 913183-12-7
• Molecular Formula: C₇₂H₇₀INO₄
• Molecular Weight: 1140.26
• Mol file: 913183-12-7.mol

Synonyms:N-(2,6-diisopropylphenyl)-1,6-bis[4-(1,1,3,3-tetramethylbutyl)phenoxy]-11-iodoterrylene-3,4-dicarboximide

Chemical Property of N-(2,6-diisopropylphenyl)-1,6-bis[4-(1,1,3,3-tetramethylbutyl)phenoxy]-11-iodoterrylene-3,4-dicarboximide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(2,6-diisopropylphenyl)-1,6-bis[4-(1,1,3,3-tetramethylbutyl)phenoxy]-11-iodoterrylene-3,4-dicarboximide

There total 1 articles about N-(2,6-diisopropylphenyl)-1,6-bis[4-(1,1,3,3-tetramethylbutyl)phenoxy]-11-iodoterrylene-3,4-dicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

N-(2,6-diisopropylphenyl)-1,6-bis[4-(1,1,3,3-tetramethylbutyl)phenoxy]-11-aminoterrylene-3,4-dicarboximide → N-(2,6-diisopropylphenyl)-1,6-bis[4-(1,1,3,3-tetramethylbutyl)phenoxy]-11-iodoterrylene-3,4-dicarboximide (913183-12-7)

Guidance literature:

N-(2,6-diisopropylphenyl)-1,6-bis[4-(1,1,3,3-tetramethylbutyl)phenoxy]-11-aminoterrylene-3,4-dicarboximide; With hydrogenchloride; sodium nitrite; In tetrahydrofuran; diethyl ether; water; acetonitrile; at -10 - -5 ℃; for 0.75h;

With sodium iodide; In tetrahydrofuran; diethyl ether; water; acetonitrile; at 0 - 20 ℃;

Reference yield: 85.0%

N-(2,6-diisopropylphenyl)-1,6-bis[4-(1,1,3,3-tetramethylbutyl)phenoxy]-11-iodoterrylene-3,4-dicarboximide (913183-12-7) + N-(2,6-diisopropylphenyl)-1,6-bis[4-(1,1,3,3-tetramethyl-butyl)phenoxy]-11-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)terrylene-3,4-dicarbocylic acid imide → bis[N-(2,6-diisopropylphenyl)-1,6-bis[4-(1,1,3,3-tetramethyl-butyl)phenoxy]-11-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)terrylene-3,4-dicarbocylic acid imide]

Guidance literature:

With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; ethanol; water; at 70 ℃; for 24h;

Reference yield: 78.0%

N-(2,6-diisopropylphenyl)-1,6-bis[4-(1,1,3,3-tetramethylbutyl)phenoxy]-11-iodoterrylene-3,4-dicarboximide (913183-12-7) + bis(pinacol)diborane (73183-34-3) → N-(2,6-diisopropylphenyl)-1,6-bis[4-(1,1,3,3-tetramethyl-butyl)phenoxy]-11-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)terrylene-3,4-dicarbocylic acid imide

Guidance literature:

With potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In toluene; at 60 ℃;

Downstream raw materials:

N-(2,6-diisopropylphenyl-1,6-bis-[4-(1,1,3,3-tetramethyl-butyl)-phenoxy]-11-(9-[N-(2,6-diisopropylphenyl)]-1,6-bis[4-(1,1,3,3-tetramethyl-butyl)-phenoxy]perylene-3,4-dicarboxylic acid imide)terrylene-3,4-dicarboxylic acid) imide