(O-benzyl-L-tyrosyl)-N'-nitro-L-arginine benzyl ester

Base Information

Chemical Name:(O-benzyl-L-tyrosyl)-N'-nitro-L-arginine benzyl ester
CAS No.:85479-40-9
Molecular Formula:C₄₀H₅₂N₈O₁₀S
Molecular Weight:836.966
Hs Code.:

<N-tert-butyloxycarbonyl-S-(acetamidomethyl)-L-cysteinyl>(O-benzyl-L-tyrosyl)-N'-nitro-L-arginine benzyl ester

Synonyms:(O-benzyl-L-tyrosyl)-N'-nitro-L-arginine benzyl ester

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Chemical Property of (O-benzyl-L-tyrosyl)-N'-nitro-L-arginine benzyl ester

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Technology Process of (O-benzyl-L-tyrosyl)-N'-nitro-L-arginine benzyl ester

There total 4 articles about (O-benzyl-L-tyrosyl)-N'-nitro-L-arginine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2130-96-3,54784-43-9
O-benzyl-N-tert-butoxycarbonyl-L-tyrosine

: 85479-40-9
(O-benzyl-L-tyrosyl)-N'-nitro-L-arginine benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) N-methylmorpholine, isobutyl chloroformate / 1.) DMF, 20 min, 2.) -20 deg C, 3 h

2: 94 percent / HCl / dioxane / 0.5 h / Ambient temperature

3: 1.) isobutyl chloroformate, N-methylmorpholine / 1.) DMF, 25 min, 2.) -25 deg C, 3 h

With 4-methyl-morpholine; hydrogenchloride; isobutyl chloroformate; In 1,4-dioxane;
DOI:10.1021/ja00350a054

Reference yield:

: 7672-27-7
N'-nitro-L-arginine benzyl ester

: 85479-40-9
(O-benzyl-L-tyrosyl)-N'-nitro-L-arginine benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) N-methylmorpholine, isobutyl chloroformate / 1.) DMF, 20 min, 2.) -20 deg C, 3 h

2: 94 percent / HCl / dioxane / 0.5 h / Ambient temperature

3: 1.) isobutyl chloroformate, N-methylmorpholine / 1.) DMF, 25 min, 2.) -25 deg C, 3 h

With 4-methyl-morpholine; hydrogenchloride; isobutyl chloroformate; In 1,4-dioxane;
DOI:10.1021/ja00350a054

Reference yield:

: 85479-38-5
(N-tert-butyloxycarbonyl-O-benzyl-L-tyrosyl)-N'-nitro-L-arginine benzyl ester

: 85479-40-9
(O-benzyl-L-tyrosyl)-N'-nitro-L-arginine benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / HCl / dioxane / 0.5 h / Ambient temperature

2: 1.) isobutyl chloroformate, N-methylmorpholine / 1.) DMF, 25 min, 2.) -25 deg C, 3 h

With 4-methyl-morpholine; hydrogenchloride; isobutyl chloroformate; In 1,4-dioxane;
DOI:10.1021/ja00350a054