C₄₉H₅₆O₁₀SSi

Base Information

Chemical Name:C₄₉H₅₆O₁₀SSi
CAS No.:220690-94-8
Molecular Formula:C₄₉H₅₆O₁₀SSi
Molecular Weight:865.129
Hs Code.:

C<sub>49</sub>H<sub>56</sub>O<sub>10</sub>SSi

Synonyms:C₄₉H₅₆O₁₀SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₉H₅₆O₁₀SSi

Chemical Property:

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Technology Process of C₄₉H₅₆O₁₀SSi

There total 20 articles about C₄₉H₅₆O₁₀SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 220691-92-9
C₄₉H₅₆O₈SSi

: 220690-94-8
C₄₉H₅₆O₁₀SSi

Guidance literature:: With sodium acetate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃;

Reference yield:

: 52813-63-5
(5R)-2,3,4,5-tetrahydro-5-hydroxymethyl-2-furanone

: 220690-94-8
C₄₉H₅₆O₁₀SSi

Guidance literature:: Multi-step reaction with 8 steps

1: 84 percent / Ph₃P, DEAD / tetrahydrofuran / Heating

2: 98 percent / DIBAL-H / toluene / -78 °C

3: acetonitrile

4: NaOH / H₂O / Heating

5: 1.) LDA, 2.) t-BuOK / 1.) THF, -78 deg C, 2.) THF, -78 deg C to r.t.

6: H₂O, TFA / CH₂Cl₂

7: 87 percent / imidazole / dimethylformamide

8: 96 percent / MCPBA, NaOAc / CH₂Cl₂ / 0 °C

With 1H-imidazole; sodium hydroxide; potassium tert-butylate; water; sodium acetate; diisobutylaluminium hydride; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; trifluoroacetic acid; lithium diisopropyl amide; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 7217-59-6
2-Methoxybenzenethiol

: 220690-94-8
C₄₉H₅₆O₁₀SSi

Guidance literature:: Multi-step reaction with 11 steps

1: 87 percent / BF₃*Et₂O / CH₂Cl₂

2: 100 percent / K₂CO₃, MeOH

3: 68 percent / CSA / methanol / Heating

4: 95 percent / NaH / dimethylformamide

5: Et₃N / CH₂Cl₂ / -78 °C

6: dimethylformamide; acetonitrile

7: 90 percent / DIBAL-H / toluene / -78 °C

8: 1.) LDA, 2.) t-BuOK / 1.) THF, -78 deg C, 2.) THF, -78 deg C to r.t.

9: H₂O, TFA / CH₂Cl₂

10: 87 percent / imidazole / dimethylformamide

11: 96 percent / MCPBA, NaOAc / CH₂Cl₂ / 0 °C

With 1H-imidazole; methanol; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; potassium tert-butylate; water; sodium acetate; sodium hydride; diisobutylaluminium hydride; potassium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; lithium diisopropyl amide; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;